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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List picromycin

picromycin synthesis

1synthesis methods
Oxacyclotetradec-11-ene-2,4,10-trione, 6-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-14-ethyl-13-hydroxy-3,5,7,9,13-pentamethyl-, (3R,5R,6S,7S,9R,11E,13S,14R)-

77659-32-6
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picromycin

19721-56-3
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Yield:19721-56-3 91%

Reaction Conditions:

with water;triethylamine in methanol at 20; for 3 h;

References:

Oh, Hong-Se;Kang, Han-Young [Journal of Organic Chemistry,2012,vol. 77,# 2,p. 1125 - 1130] Location in patent:experimental part

picromycin Related Search:

Ethyl isobutyrylacetate METHYL-(TETRAHYDRO-PYRAN-4-YL)-AMINE HCL Methyl isobutyrylacetate FEMA 2200 Ethyl butyrylacetate 4-Aminotetrahydropyran 6-METHYL-3-OXO-HEPTANOIC ACID ETHYL ESTER 3-ISOBUTOXY PROPYLAMINE 3-De[(2,6-dideoxy-3-C-methyl-3-O-methyl-a-L-ribo-hexopyranosyl)oxy]-10,11-didehydro-11-deoxy-6-O-methyl-3-oxo-erythromycin 2'-acetate