ChemicalBook--->CAS DataBase List--->1131-60-8

1131-60-8

1131-60-8 Structure

1131-60-8 Structure
IdentificationMore
[Name]

4-Cyclohexylphenol
[CAS]

1131-60-8
[Synonyms]

4-CYCLOHEXYLPHENOL
4-HYDROXYPHENYLCYCLOHEXANE
CYCLOHEXYL PHENOL
P-CYCLOHEXYLPHENOL
4-cyclohexyl-pheno
Phenol, p-cyclohexyl-
p-Hydroxyphenylcyclohexane
CYCLOHEXYLPHENOL, 4-
PARA-CYCLOHEXYLPHENOL
4-(Cyclohexane-1-yl)phenol
[EINECS(EC#)]

214-465-4
[Molecular Formula]

C12H16O
[MDL Number]

MFCD00035699
[Molecular Weight]

176.25
[MOL File]

1131-60-8.mol
Chemical PropertiesBack Directory
[Melting point ]

130-135°C
[Boiling point ]

213-215°C
[density ]

0.9452 (rough estimate)
[vapor pressure ]

0.823-3.6Pa at 25℃
[refractive index ]

1.5415 (estimate)
[storage temp. ]

Inert atmosphere,Room Temperature
[form ]

Solid:flakes
[pka]

10.15±0.13(Predicted)
[color ]

White to Light yellow to Light orange
[Water Solubility ]

66.66mg/L(25 ºC)
[Dielectric constant]

4.0(54℃)
[LogP]

4.22-4.33
[CAS DataBase Reference]

1131-60-8(CAS DataBase Reference)
[NIST Chemistry Reference]

Phenol, 4-cyclohexyl-(1131-60-8)
[EPA Substance Registry System]

1131-60-8(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
[Hazard Note ]

Irritant
[HS Code ]

2907199090
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

4-Cyclohexylphenol(1131-60-8).msds
Hazard InformationBack Directory
[Uses]

4-Cyclohexylphenol is a derivative of Cyclohexylphenol (CHP), which is widely used in the preparation of dyes, resins, and biocides[2]. 4-Cyclohexylphenol labelled with 35s can be used for metabolic studies[3].
[Synthesis]

4-Cyclohexylphenol is obtained by hydroalkylation of phenol using phenol as a raw material in the presence of a palladium catalyst and a molten salt (NaCl-AlCl3)[1]. The specific synthesis steps are as follows:
The hydroalkylation of phenol in the presence of palladium catalyst and fused salt (NaCl-AlCl3) under hydrogen pressure was carried out. By using 1% Pd-Al2O3 (1 g) and the fused salt (1 : 1 mol ratio, 6 g), 4-cyclohexylphenol was obtained selectively from 1 (30 g) in a yield of 31.9% at 120°C for 4.5 h.
[References]

[1] T. KAMIYAMA; M. I; S Enomoto. Hydroalkylation of phenol to cyclohexylphenol in the presence of Pd-Al2O3 and NaCl-AlCl3 under hydrogen pressure.[J]. Chemical & pharmaceutical bulletin, 1986. DOI:10.1248/CPB.34.450.
[2] S. GUTIéRREZ-RUBIO . Synthesis of cyclohexylphenol via phenol hydroalkylation using Co2P/zeolite catalysts[J]. Catalysis Today, 2022. DOI:10.1016/j.cattod.2021.11.039.
[3] D.J. HEARSE; Gillian M P; A H Olavesen. The preparation and characterization of a series of 35S-labelled aryl sulphate esters for metabolic studies[J]. Biochemical pharmacology, 1969. DOI:10.1016/0006-2952(69)90022-7.
Spectrum DetailBack Directory
[Spectrum Detail]

4-Cyclohexylphenol(1131-60-8)MS
4-Cyclohexylphenol(1131-60-8)1HNMR
4-Cyclohexylphenol(1131-60-8)13CNMR
4-Cyclohexylphenol(1131-60-8)IR1
4-Cyclohexylphenol(1131-60-8)IR2
4-Cyclohexylphenol(1131-60-8)Raman
Well-known Reagent Company Product InformationBack Directory
[TCI AMERICA]

4-Cyclohexylphenol,>95.0%(GC)(1131-60-8)
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