Identification | Back Directory | [Name]
androstane | [CAS]
24887-75-0 | [Synonyms]
Androstane (van) 1H-Cyclopenta(A)phenanthrene, hexadecahydro-10,13-dimethyl-, (8S-(8alpha,9beta,10alpha,13alpha,14beta))- | [Molecular Formula]
C19H32 | [MOL File]
24887-75-0.mol | [Molecular Weight]
260.46 |
Hazard Information | Back Directory | [Definition]
ChEBI:Androstane is a steroid fundamental parent. | [Purification Methods]
Purify 5-androstane by chromatography through Al2O3 (grade III) and elute with pet ether and recrystallise from MeOH (2x) and Me2CO/MeOH. It sublimes at 60o/high vacuum. Also dissolve it in pet ether, filter it through silica gel, evaporate and recrystallise it. [Steiger & Reichstein Helv Chim Acta 20 817 1937, Prelog et al. Helv Chim Acta 27 66 1944, IR, NMR: Halkes & Havinga Rec Trav Chim Pays-Bas 8 4 889 1965, Allinger et al. Tetrahedron 27 5073 1971, Beilstein 5 III 1110, 5 IV 1211.] |
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