ChemicalBook--->CAS DataBase List--->4477-28-5

4477-28-5

4477-28-5 Structure

4477-28-5 Structure
IdentificationMore
[Name]

4-Diazodiphenylamine sulfate
[CAS]

4477-28-5
[Synonyms]

1,4-DIAZODIPHENYLAMINE HYDROGEN SULFATE
4-AMINO-DIPHENYLAMINE, DIAZONIUM SALT
4-AMINODIPHENYLAMINE DIAZONIUM SULFATE
4-DIAZODIPHENYLAMINE SULFATE
4-(N-PHENYLAMINO)BENZENEDIAZONIUM HYDROGENSULFATE
4-(PHENYLAMINO)BENZENEDIAZONIUM SULFATE
AZOIC DIAZO NO 22
CI 37240
DIAZO S
DIPHENYLAMINE-4-DIAZONIUM SULFATE
FAST BLUE SALT R
P-AMINODIPHENYLAMINE DIAZONIUM SULFATE
P-(PHENYLAMINO)BENZENEDIAZONIUM SULFATE
VARIAMINE BLUE RT SALT
4-(phenylamino)-benzenediazoniusulfate(1:1)
AcnaBlueRTSalt
BluebaseRT
BlueSaltNR
C.I.AzoicDiazoComponent22(37240)
DaitoBlueSaltVR
[EINECS(EC#)]

224-756-8
[Molecular Formula]

C24H22N8O4S
[MDL Number]

MFCD00011895
[Molecular Weight]

518.55
[MOL File]

4477-28-5.mol
Chemical PropertiesBack Directory
[Boiling point ]

623.17℃[at 101 325 Pa]
[density ]

1.512[at 20℃]
[vapor pressure ]

0Pa at 25℃
[Colour Index ]

37240
[Water Solubility ]

21.24g/L at 20℃
[LogP]

1.28 at 23℃
[CAS DataBase Reference]

4477-28-5(CAS DataBase Reference)
[EPA Substance Registry System]

4477-28-5(EPA Substance)
Safety DataBack Directory
[WGK Germany ]

3
[HS Code ]

2927.00.5000
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Sodium nitrite-->Sodium sulfide-->4-Chloronitrobenzene-->Diphenylamine-->4-Aminodiphenylamine-->4-NITROSODIPHENYLAMINE
Spectrum DetailBack Directory
[Spectrum Detail]

4-Diazodiphenylamine sulfate(4477-28-5)IR1
4-Diazodiphenylamine sulfate(4477-28-5)IR2
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

4477-28-5(sigmaaldrich)
[TCI AMERICA]

4-Diazodiphenylamine Sulfate,>98.0%(T)(4477-28-5)
Hazard InformationBack Directory
[Flammability and Explosibility]

Notclassified
[Purification Methods]

Dissolve 10g of the dye in 100mL of hot water. Sodium dithionite (0.4g) is then added, followed by active carbon (1.5g) and is filtered hot. To the colourless or slightly yellow filtrate a solution of saturated NaCl is added, and the mixture is cooled. The needles are filtered off, washed with cold water, dried at room temperature, and stored in a dark bottle (light sensitive). [Anderson & Steedly J Am Chem Soc 76 5144 1954, Erdey Chem Analyst 48 106 1959, Beilstein 16 H 602, 16 I 371, 16 II 307, 16 III 575. ]
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