Methyl 3-(cyanomethyl)benzoate
- CAS No.
- 68432-92-8
- Chemical Name:
- Methyl 3-(cyanomethyl)benzoate
- Synonyms
- METHYL 3-(CYANOMETHYL) BENZOATE;Famoxadone Impurity 13;Methyl m-(cyanomethyl)benzoate;3-(Cyanomethyl)benzoate methyl ester;3-CYANOMETHYLBENZOIC ACID METHYL ESTER;Benzoicacid, 3-(cyanomethyl)-, methyl ester;high quality 3-CYANOMETHYLBENZOIC ACID METHYL ESTER
- CBNumber:
- CB1757286
- Molecular Formula:
- C10H9NO2
- Molecular Weight:
- 175.18
- MDL Number:
- MFCD07783720
- MOL File:
- 68432-92-8.mol
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P264-P280-P302+P352-P321-P332+P313-P362-P264-P280-P305+P351+P338-P337+P313P |
| HazardClass | IRRITANT |
| HS Code | 2926907090 |
Methyl 3-(cyanomethyl)benzoate price
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | M338090 | Methyl3-(cyanomethyl)benzoate | 68432-92-8 | 1g | $75 | 2021-12-16 | Buy |
| TRC | M338090 | Methyl3-(cyanomethyl)benzoate | 68432-92-8 | 250mg | $55 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC70223 | 3-Cyanomethylbenzoic acid methyl ester | 68432-92-8 | 100g | $60 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | API0005061 | METHYL 3-(CYANOMETHYL)BENZOATE 95.00% | 68432-92-8 | 25G | $2177.18 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC70223 | 3-Cyanomethylbenzoic acid methyl ester | 68432-92-8 | 1kg | $300 | 2021-12-16 | Buy |
Methyl 3-(cyanomethyl)benzoate Chemical Properties,Uses,Production
Uses
Methyl 3-(cyanomethyl)benzoate is used as an intermediate in organic synthesis for the preparation of other compounds such as 3-(cyanomethyl)benzoic acid.
Synthesis
Methyl 3-(cyanomethyl)benzoate is synthesised using Methyl 3-(bromomethyl)benzoate as raw material by chemical reaction. The specific synthesis steps are as follows:
(i) To a solution of methyl 3-bromobenzoate (10.0 g, 44 mmol) in acetonitrile (100 mL) were added potassium cyanide (5.7 g, 87 mmol) and 18-crown-6 (1.0 g), and the mixture was stirred at room temperature for 3 days. The reaction mixture was filtered, and the solvent was evaporated under reduced pressure. The residue was purified by silica gel column chromatography (ethyl acetate/hexane=5/95-->30/70), and the fraction containing the object product was concentrated under reduced pressure to give the title compound (7.0 g, 91percent) as a colorless oil. 1H-NMR (DMSO-d6, 300 MHz) δ 3.88 (3H, s), 4.17 (2H, s), 7.57 (1H, t, J = 7.6 Hz), 7.61 - 7.69 (1H, m), 7.88 - 7.95 (1H, m), 7.97 (1H, br s).
Methyl 3-(cyanomethyl)benzoate Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18657 | 58 |
| Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | info@tianfuchem.com | China | 21667 | 55 |
| Zjartschem | +86-571 87238903 | jocelynpan@zjarts.com | CHINA | 993 | 58 |
| Changzhou Ansciep Chemical Co., Ltd. | +86 519 86305871 | sales@ansciepchem.com | CHINA | 4242 | 58 |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10312 | 58 |
| Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | sales@chemdad.com | China | 39916 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63711 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49392 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21149 | 58 |
| Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 | sale04@alfachem.cn | China | 13260 | 58 |
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