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1-BROMO-3-CHLORO-5-METHOXYBENZENE

1-BROMO-3-CHLORO-5-METHOXYBENZENE structure

CAS No.: 174913-12-3

Chemical Name:: 1-BROMO-3-CHLORO-5-METHOXYBENZENE

Synonyms: 3-Bromo-5-chloroanisole;Phloroglucinol Impurity 56;Phloroglucinol Impurity 34;1-BROMO-3-CHLORO-5-METHOXYBENZENE;Benzene, 1-bromo-3-chloro-5-methoxy-;3-bromo-5-chlorotrifluoromethoxybenzene;1-BROMO-3-CHLORO-5-METHOXYBENZENE ISO 9001：2015 REACH

CBNumber:: CB32455168

Molecular Formula:: C7H6BrClO

Molecular Weight:: 221.48

MDL Number:: MFCD11035921

MOL File:: 174913-12-3.mol

Last updated:2024-09-27 09:18:45

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1-BROMO-3-CHLORO-5-METHOXYBENZENE Properties

Boiling point	236.5±20.0 °C(Predicted)
Density	1.564±0.06 g/cm3(Predicted)
storage temp.	Sealed in dry,Room Temperature

SAFETY

Risk and Safety Statements

Symbol(GHS)	GHS07
Signal word	Warning
Hazard statements	H302-H315-H319-H332-H335
Precautionary statements	P261-P280-P305+P351+P338
HS Code	2909303890

1-BROMO-3-CHLORO-5-METHOXYBENZENE price More Price(32)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
TRC	B683568	3-Bromo-5-chloroanisole	174913-12-3	100mg	$45	2021-12-16	Buy
TRC	B683568	3-Bromo-5-chloroanisole	174913-12-3	500mg	$55	2021-12-16	Buy
AK Scientific	W3821	1-Bromo-3-chloro-5-methoxybenzene	174913-12-3	25g	$237	2021-12-16	Buy
Apolloscientific	OR400559	3-Bromo-5-chloroanisole	174913-12-3	25g	$269	2021-12-16	Buy
Matrix Scientific	076555	1-Bromo-3-chloro-5-methoxybenzene 95+%	174913-12-3	25g	$149	2021-12-16	Buy

Product number	Packaging	Price	Buy
B683568	100mg	$45	Buy
B683568	500mg	$55	Buy
W3821	25g	$237	Buy
OR400559	25g	$269	Buy
076555	25g	$149	Buy

1-BROMO-3-CHLORO-5-METHOXYBENZENE Chemical Properties,Uses,Production

Uses

1-Bromo-3-chloro-5-methoxybenzene is a commonly used organobenzene compound whose bromine or chlorine atoms on the benzene ring structure can be replaced by other halogenated atoms for the synthesis of other halogenated methoxybenzene derivatives. It can also be used to synthesise 3-Bromo-5-chlorophenol and its derivatives.

Synthesis

1-Bromo-3-chloro-5-methoxybenzene is prepared by the reaction of 1-bromo-3-chloro-5-fluoro-benzene and Sodium methanolate. The specific synthesis steps are as follows:
A solution of 1-bromo-3-chloro-5-fluoro-benzene (42a, 55 g, 263 mmol) was cooled to 0° C. and treated with a 25percent methanolic sodium methoxide solution (68 mL, 315 mmol) and heated to 40° C. for 3 h. The solution was cooled and partitioned between water (1 L) and a 1:1 mixture of hexane/diethyl ether (3.x.200 mL). The combined extracts were washed with brine (60 mL), dried (Na2SO4), filtered and the solvents evaporated in vacuo to afford 42b as an oil (57.3 g, 92percent pure, 238 mmol). The ether 42b (43 g, 173 mmol) was treated with glacial HOAc (150 mL) and 48percent aqueous HBr (100 mL) and heated to 120° C. After 40 h, the volatiles were removed while heated to 80° C. and then cooled to RT. The residue was partitioned between water (100 mL) and DCM (3.x.250 mL). The combined extracts were washed with H2O (50 mL), aqueous NaHCO3solution (2.x.50 mL), brine (50 mL), and (MgSO4). The solvents were removed to afford 23.3 g of 1-Bromo-3-chloro-5-methoxybenzene as a grey solid.

1-BROMO-3-CHLORO-5-METHOXYBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

4-chloro-3-methoxybenzenethiol 3'-Chloro-5'-methoxyacetophenone

1-BROMO-3-CHLORO-5-METHOXYBENZENE Suppliers

Global( 132)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Henan Fengda Chemical Co., Ltd	+86-371-86557731 +86-13613820652	info@fdachem.com	China	20283	58
Frapp's ChemicalNFTZ Co., Ltd.	+86 (576) 8169-6106	sales@frappschem.com	China	880	50
Capot Chemical Co.,Ltd.	+86-（0）57185586718 +86-13336195806	sales@capot.com	China	29791	60
ATK CHEMICAL COMPANY LIMITED	+undefined-21-51877795	ivan@atkchemical.com	China	32956	60
career henan chemical co	+86-0371-86658258 +8613203830695	sales@coreychem.com	China	29880	58
Changzhou Ansciep Chemical Co., Ltd.	+86 519 86305871	sales@ansciepchem.com	CHINA	4241	58
Shenzhen Nexconn Pharmatechs Ltd	+86-755-89396905 +86-15013857715	admin@nexconn.com	China	10311	58
Nanjing Dolon Biotechnology Co.,Ltd.	18905173768	sales@dolonchem.com	CHINA	2972	58
Chongqing Chemdad Co., Ltd	+86-023-6139-8061 +86-86-13650506873	sales@chemdad.com	China	39894	58
Alchem Pharmtech,Inc.	8485655694	sales@alchempharmtech.com	United States	63687	58

Supplier	Advantage
Henan Fengda Chemical Co., Ltd	58
Frapp's ChemicalNFTZ Co., Ltd.	50
Capot Chemical Co.,Ltd.	60
ATK CHEMICAL COMPANY LIMITED	60
career henan chemical co	58
Changzhou Ansciep Chemical Co., Ltd.	58
Shenzhen Nexconn Pharmatechs Ltd	58
Nanjing Dolon Biotechnology Co.,Ltd.	58
Chongqing Chemdad Co., Ltd	58
Alchem Pharmtech,Inc.	58

View Lastest Price from 1-BROMO-3-CHLORO-5-METHOXYBENZENE manufacturers

Image	Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
	2024-01-02	1-Bromo-3-chloro-5-methoxybenzene 174913-12-3	US $200.00-1.00 / KG	1KG	99%, 99.5% Sublimated	g-kg-tons, free sample is available	Henan Fengda Chemical Co., Ltd
	2019-07-06	1-BROMO-3-CHLORO-5-METHOXYBENZENE 174913-12-3	US $2.00 / kg	1kg	99%	100kg	Career Henan Chemical Co

1-Bromo-3-chloro-5-methoxybenzene
174913-12-3
US $200.00-1.00 / KG
99%, 99.5% Sublimated
Henan Fengda Chemical Co., Ltd

1-BROMO-3-CHLORO-5-METHOXYBENZENE
174913-12-3
US $2.00 / kg
99%
Career Henan Chemical Co

174913-12-3(1-BROMO-3-CHLORO-5-METHOXYBENZENE)Related Search:

2-Bromo-4-chloro-6-fluorotoluene 3-Bromo-2-iodotoluene 2-BROMO-4-METHYLBENZOTRIFLUORIDE 3-fluoro-5-iodobenzodifluoride 1-BROMO-2,3-DIFLUORO-5-METHYLBENZENE

2-BROMO-4-CHLORO-6-NITROTOLUENE 2-bromo-6-chloro-3-fluorotoluene 2,6-Dichloro-4-fluorobenzotrifluoride 2-Chloro-3-fluorobenzotrifluoride 2,6-Dibromobenzotrifluoride

2-CHLORO-4-FLUOROBENZOTRIFLUORIDE 2,4-Dibromo-6-fluorotoluene 3-Bromo-5-chlorophenol 2-Chloro-4-bromo-6-trifluoromethoxyaniline 4-bromo-6-chlorobenzo[d]oxazol-2(3H)-one

1-BROMO-3-CHLORO-5-METHOXYBENZENE

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1-BROMO-3-CHLORO-5-METHOXYBENZENE 3-Bromo-5-chloroanisole Benzene, 1-bromo-3-chloro-5-methoxy- Phloroglucinol Impurity 34 3-bromo-5-chlorotrifluoromethoxybenzene 1-BROMO-3-CHLORO-5-METHOXYBENZENE ISO 9001：2015 REACH Phloroglucinol Impurity 56 174913-12-3