ChemicalBook >> CAS DataBase List >>2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester
- CAS No.
- 1882074-17-0
- Chemical Name:
- 2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester
- Synonyms
- 2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester
- CBNumber:
- CB38372957
- Molecular Formula:
- C21H20O5
- Molecular Weight:
- 352.38
- MDL Number:
- MOL File:
- 1882074-17-0.mol
Last updated:2022-11-14 17:31:25
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Chemical Properties,Uses,Production
Preparation
The preparation of 2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester is as follows:1: Methacrylic acid (3.56 g, 41.5 mmol) and 4-(dimethylamino)pyridine (0.17 g, 1.4 mmol) is added to a suspension of 1b (3.0 g, 13.9 mmol) in 40 ml dichloromethane. The reaction mixture is treated dropwise at 0° C. with a solution of N-(3-dimethylaminopropyl)-N′-ethylcarbodiimide (6.44 g, 41.5 mmol) in dichloromethane (20 ml) and stirred for 20 h at room temperature. After removing solvent in vacuo, the oily residue is purified by silica gel chromatography with dichloromethane/ethyl acetate 20:1 as eluent. The obtained product is recrystallized from acetonitril to afford white crystals of 1 (2.1 g, mp. 105° C.).
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Preparation Products And Raw materials
Raw materials
Preparation Products
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester Suppliers
Global( 1)Suppliers
Supplier | Tel | Country | ProdList | Advantage | |
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Univar Solutions(China) Co., Ltd. | +8615902132654 | ivy.zhuang@univarsolutions.com | China | 654 | 58 |
Supplier | Advantage |
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Univar Solutions(China) Co., Ltd. | 58 |
1882074-17-0(2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester)Related Search:
2-Propenoic acid, 2-methyl-, 1,1'-(2-methoxy[1,1'-biphenyl]-4,4'-diyl) ester
1882074-17-0