7-Nitro-1,2,3,4-tetrahydroquinoline
- CAS No.
- 30450-62-5
- Chemical Name:
- 7-Nitro-1,2,3,4-tetrahydroquinoline
- Synonyms
- 7-Nitro-1;7-Nitro-1,2,3,4-Terahydroquinoline;7-NITRO-1,2,3,4-TETRAHYDROQUINOLINE;1,2,3,4-TETRAHYDRO-7-NITROQUINOLINE;7-Nitro-1,2,3,4-tetrahydroquinoline>Quinoline, 1,2,3,4-tetrahydro-7-nitro-;7-Nitro-1,2,3,4-tetrahydroquinoline,95%;7-NITRO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE;7-Nitro-1,2,3,4-tetrahydroquinoline 1,2,3,4-Tetrahydro-7-nitroquinoline
- CBNumber:
- CB6246251
- Molecular Formula:
- C9H10N2O2
- Molecular Weight:
- 178.19
- MDL Number:
- MFCD00496654
- MOL File:
- 30450-62-5.mol
Melting point | 61.0 to 65.0 °C |
---|---|
Boiling point | 325.2±31.0 °C(Predicted) |
Density | 1.236±0.06 g/cm3(Predicted) |
storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
solubility | soluble in Methanol |
pka | 3.44±0.20(Predicted) |
form | Powder |
color | Red |
CAS DataBase Reference | 30450-62-5(CAS DataBase Reference) |
7-Nitro-1,2,3,4-tetrahydroquinoline price More Price(31)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich | MNO000018 | 7-Nitro-1,2,3,4-tetrahydroquinoline Aldrich | 30450-62-5 | 1g | $70.9 | 2024-03-01 | Buy |
TCI Chemical | N0955 | 7-Nitro-1,2,3,4-tetrahydroquinoline >98.0%(GC)(T) | 30450-62-5 | 5g | $77 | 2024-03-01 | Buy |
TCI Chemical | N0955 | 7-Nitro-1,2,3,4-tetrahydroquinoline >98.0%(GC)(T) | 30450-62-5 | 25g | $249 | 2024-03-01 | Buy |
Alfa Aesar | H61612 | 7-Nitro-1,2,3,4-tetrahydroquinoline, 95% | 30450-62-5 | 1g | $41.65 | 2024-03-01 | Buy |
Alfa Aesar | H61612 | 7-Nitro-1,2,3,4-tetrahydroquinoline, 95% | 30450-62-5 | 5g | $179.65 | 2024-03-01 | Buy |
7-Nitro-1,2,3,4-tetrahydroquinoline Chemical Properties,Uses,Production
Uses
7-Nitro-1,2,3,4-tetrahydroquinoline is a quinoline compound that can be used as a reagent in chemical reactions or as an intermediate in organic synthesis. It can be used to prepare 7-Aminoquinoline and 7-Nitroquinoline.
Synthesis
7-Nitro-1,2,3,4-tetrahydroquinoline is synthesised by the reaction of 1,2,3,4-tetrahydroquinoline and nitric acid in sulphuric acid solution. The specific synthesis steps are as follows:
Concentrated sulfuric acid (30.00 mL) was cooled to -10° C. with an ice/salt bath.
To this, 1,2,3,4-tetrahydro-quinoline (10.60 g, 75.60 mmol) and a solution of nitric acid (99.5percent, 4.80 g, 75.60 mmol) in sulfuric acid (15.00 mL) were added simultaneously within 1 hour, so that the temperature of the reaction mixture does not exceed 10° C.
The mixture was stirred then for 2.5 hours at -5° C., then poured over ice and treated with sodium carbonate (0.10 kg) until pH 8-9 was reached.
The solid was filtered, washing with water, then dissolved in dichloromethane.
The organic phase was washed with water, dried over magnesium sulphate and evaporated.
7-Nitro-1,2,3,4-tetrahydro-quinoline was obtained as a viscous brown oil, 13.70 g (85percent), 84percent purity.
7-Nitro-1,2,3,4-tetrahydroquinoline Preparation Products And Raw materials
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 | info@spring-chem.com | China | 2068 | 57 |
Capot Chemical Co.,Ltd. | +86-(0)57185586718 +86-13336195806 | sales@capot.com | China | 29791 | 60 |
Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10310 | 58 |
Shanghai Worldyang Chemical Co.,Ltd. | +86-021-56795779 +8613651600618 | sales@worldyachem.com | China | 1243 | 58 |
Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49374 | 58 |
career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29811 | 58 |
SIMAGCHEM CORP | +86-13806087780 | sale@simagchem.com | China | 17365 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
Jinjiangchem Corporation | 512-50133713 | sales@jinjiangchem.com | CHINA | 1072 | 58 |
View Lastest Price from 7-Nitro-1,2,3,4-tetrahydroquinoline manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2024-11-27 | 7-Nitro-1,2,3,4-tetrahydroquinoline
30450-62-5
|
US $0.00 / G | 10G | 98%min | 300KG/month | WUHAN FORTUNA CHEMICAL CO., LTD | ||
2019-12-26 | 1,2,3,4-TETRAHYDRO-7-NITROQUINOLINE
30450-62-5
|
US $1.00 / KG | 1KG | 99% | 100KG | Career Henan Chemical Co |
- 7-Nitro-1,2,3,4-tetrahydroquinoline
30450-62-5
- US $0.00 / G
- 98%min
- WUHAN FORTUNA CHEMICAL CO., LTD
- 1,2,3,4-TETRAHYDRO-7-NITROQUINOLINE
30450-62-5
- US $1.00 / KG
- 99%
- Career Henan Chemical Co
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