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4-Iodoanisole

CAS No.
696-62-8
Chemical Name:
4-Iodoanisole
Synonyms
1-IODO-4-METHOXYBENZENE;P-IODOANISOLE;4-IODOANISOL;Isoform;4-IODANISOLE;p-iodoanisol;4-lodoanisole;4-METHOXYIODOBENZENE;CREM-α;4-iodoether
CBNumber:
CB6450614
Molecular Formula:
C7H7IO
Molecular Weight:
234.03
MDL Number:
MFCD00001056
MOL File:
696-62-8.mol
MSDS File:
SDS
Last updated:2024-12-18 14:08:57

4-Iodoanisole Properties

Melting point 50-53 °C(lit.)
Boiling point 237 °C726 mm Hg(lit.)
Density 1.7904 (estimate)
Flash point >230 °F
storage temp. Keep in dark place,Sealed in dry,Room Temperature
solubility Soluble in ethanol, ether, chloroform.
form Crystalline Powder and Chunks
color Off-white to brown
Sensitive Light Sensitive
BRN 1906692
InChIKey SYSZENVIJHPFNL-UHFFFAOYSA-N
CAS DataBase Reference 696-62-8(CAS DataBase Reference)
NIST Chemistry Reference Benzene, 1-iodo-4-methoxy-(696-62-8)
EPA Substance Registry System Benzene, 1-iodo-4-methoxy- (696-62-8)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313-P261-P280a-P304+P340-P305+P351+P338-P405-P501a
Hazard Codes  Xi,Xn
Risk Statements  36/37/38
Safety Statements  26-36-24/25
WGK Germany  3
8
TSCA  Yes
HS Code  29093090
NFPA 704
0
1 0

4-Iodoanisole price More Price(42)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich I7608 4-Iodoanisole 98% 696-62-8 25g $46.8 2024-03-01 Buy
Sigma-Aldrich I7608 4-Iodoanisole 98% 696-62-8 100g $140 2024-03-01 Buy
TCI Chemical I0378 4-Iodoanisole >99.0%(GC) 696-62-8 25g $30 2024-03-01 Buy
TCI Chemical I0378 4-Iodoanisole >99.0%(GC) 696-62-8 100g $82 2024-03-01 Buy
Alfa Aesar A12144 4-Iodoanisole, 98+% 696-62-8 25g $34.1 2024-03-01 Buy
Product number Packaging Price Buy
I7608 25g $46.8 Buy
I7608 100g $140 Buy
I0378 25g $30 Buy
I0378 100g $82 Buy
A12144 25g $34.1 Buy

4-Iodoanisole Chemical Properties,Uses,Production

Description

4-Iodoanisole (chemical formula: C7H7IO) is an organic compound being soluble in ethanol, ether and chloroform. It has a wide range of medicals industrial applications. For example, it can be used as human and animal nutrition products, antiseptics, disinfectants, pharmaceutical intermediates, polarizing films for liquid crystal display (LCD) chemicals. Its iodine derivatives can also be used as organic building blocks and analytic reagents.

References

https://www.fishersci.pt/shop/products/4-iodoanisole-98-7/11480113

Chemical Properties

off-white to brown crystalline powder and chunks. Melting point 51-52 ℃, boiling point 237 ℃ (96.8kPa). Soluble in organic solvents such as alcohol and ether, but insoluble in water. Iodine can be easily separated and analyzed by light.

Uses

4-Iodoanisole is used in wide range of medicals industrial applications as well as in human and animal nutrition products, pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals. Iodine derivatives are also used as organic building blocks, analytical reagents.

Preparation

4-Iodoanisole is synthesized by the reaction of anisole with iodine chloride. Add anisole to glacial acetic acid, stir and slowly add iodine chloride. After the addition was completed, the temperature was refluxed for 3.5h. Cool, pour into ice water, and precipitate p-iodoanisole. After it was separated, the free iodine was washed with 5% sodium sulfite, then washed with water, distilled under reduced pressure, and the fractions with a boiling point of 140-160 °C (5.33 kPa) were collected and cooled to 0 °C for filtration. Wash with methanol and recrystallize to obtain the finished product.

Definition

ChEBI: (alpha-D-mannosyl)7-beta-D-mannosyl-diacetylchitobiosyl-L-asparagine, isoform B (protein) is a member of methoxybenzenes.

Synthesis Reference(s)

The Journal of Organic Chemistry, 58, p. 2058, 1993 DOI: 10.1021/jo00060a020
Tetrahedron Letters, 27, p. 3497, 1986 DOI: 10.1016/S0040-4039(00)84832-7

Purification Methods

Crystallise 4-iodoanisole from aqueous EtOH and/or distil it under vacuum. [Beilstein 6 H 208, 6 I 109, 6 II 199, 6 III 744, 6 IV 1075.]

Global( 417)Suppliers
Supplier Tel Email Country ProdList Advantage
Hebei Weibang Biotechnology Co., Ltd
+8615531157085 abby@weibangbio.com China 8808 58
Hebei Mojin Biotechnology Co., Ltd
+86 13288715578 +8613288715578 sales@hbmojin.com China 12834 58
Henan Fengda Chemical Co., Ltd
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Henan Tianfu Chemical Co.,Ltd.
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+86-755-89396905 +86-15013857715 admin@nexconn.com China 10311 58
Chongqing Chemdad Co., Ltd
+86-023-6139-8061 +86-86-13650506873 sales@chemdad.com China 39894 58
Alchem Pharmtech,Inc.
8485655694 sales@alchempharmtech.com United States 63687 58

View Lastest Price from 4-Iodoanisole manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
4-Iodoanisole pictures 2024-11-01 4-Iodoanisole
696-62-8
US $10.00 / KG 1KG 99% 10 mt Hebei Weibang Biotechnology Co., Ltd
4-Iodoanisole pictures 2024-05-12 4-Iodoanisole
696-62-8
US $397.00 / Kg 1Kg 98 500 Kg R&D Scientific Inc.
	4-Iodoanisole pictures 2023-12-24 4-Iodoanisole
696-62-8
US $100.00-1.00 / KG 1KG 99% g-kg-tons, free sample is available Henan Fengda Chemical Co., Ltd
  • 4-Iodoanisole pictures
  • 4-Iodoanisole
    696-62-8
  • US $10.00 / KG
  • 99%
  • Hebei Weibang Biotechnology Co., Ltd
  • 	4-Iodoanisole pictures
  • 4-Iodoanisole
    696-62-8
  • US $100.00-1.00 / KG
  • 99%
  • Henan Fengda Chemical Co., Ltd
1-iodo-4-methoxy-benzen 4-Iodophenyl methyl ether, 4-Methoxyiodobenzene Methyl(4-iodophenyl) ether 4-Iodoanisole p-Iodoanisole Of iodine anisole 1-Iodo-4-methoxybenzene, 4-Iodophenyl methyl ether 4-iodoaisole 4-Iodoanisole, 98% 100GR 4-Iodoanisole, 98% 25GR 4-iodoether 4-Iodoanisole, 99.5% cAMP-responsive element modulator CREM-α 4-Iodophenyl methyl ether 4-Methoxyiodobenzene 1-Iodo-4-methoxybenzene 4-Iodomethoxybenzene 4-Methoxyphenyl iodide Anisole, 4-iodo- Anisole, p-iodo- anisole,4-iodo- p-Iodomethoxybenzene p-Iodophenyl methyl ether p-Methoxyiodobenzene p-Methoxyphenyl iodide 4-IODOANISOLE 4-IODOPHENYL METHYL ETHER AURORA KA-7366 BENZENE, 1-IODO-4-METHOXY- 4-Iodoanisole,~99% 4-Iodoanisole,98+% 4-IODOANISOLE / 1-IODO-4-METHOXYBENZENE PARA IODO ANISOLE 4-Iodoanisole> 4-lodoanisole P-IODOANISOLE 1-IODO-4-METHOXYBENZENE 4-IODANISOLE 4-IODOANISOL 4-METHOXYIODOBENZENE p-iodoanisol Isoform 4-Idiobenzyl ether Guaiacol Impurity 13 Acetylsalicylic Acid Impurity 16 696-62-8 696-42-8 IC6H4OCH3 ETHER Ethers Organic Building Blocks Oxygen Compounds Building Blocks Pyridines ,Halogenated Heterocycles Building Blocks C2 to C8 Chemical Synthesis Ethers Organic Building Blocks Oxygen Compounds