4-아이오딘아니솔
|
|
4-아이오딘아니솔 속성
- 녹는점
- 50-53 °C(lit.)
- 끓는 점
- 237 °C726 mm Hg(lit.)
- 밀도
- 1.7904 (estimate)
- 인화점
- >230 °F
- 저장 조건
- Keep in dark place,Sealed in dry,Room Temperature
- 용해도
- 에탄올, 에테르, 클로로포름에 용해됩니다.
- 물리적 상태
- 결정성 분말 및 덩어리
- 색상
- 황백색에서 갈색까지
- 감도
- Light Sensitive
- BRN
- 1906692
- InChIKey
- SYSZENVIJHPFNL-UHFFFAOYSA-N
- CAS 데이터베이스
- 696-62-8(CAS DataBase Reference)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
| 위험품 표기 | Xi,Xn | ||
|---|---|---|---|
| 위험 카페고리 넘버 | 36/37/38 | ||
| 안전지침서 | 26-36-24/25 | ||
| WGK 독일 | 3 | ||
| F 고인화성물질 | 8 | ||
| TSCA | Yes | ||
| HS 번호 | 29093090 | ||
| 기존화학 물질 | KE-05-0753 |
4-아이오딘아니솔 C화학적 특성, 용도, 생산
화학적 성질
off-white to brown crystalline powder and chunks. Melting point 51-52 ℃, boiling point 237 ℃ (96.8kPa). Soluble in organic solvents such as alcohol and ether, but insoluble in water. Iodine can be easily separated and analyzed by light.용도
4-Iodoanisole is used in wide range of medicals industrial applications as well as in human and animal nutrition products, pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals. Iodine derivatives are also used as organic building blocks, analytical reagents.제조 방법
4-Iodoanisole is synthesized by the reaction of anisole with iodine chloride. Add anisole to glacial acetic acid, stir and slowly add iodine chloride. After the addition was completed, the temperature was refluxed for 3.5h. Cool, pour into ice water, and precipitate p-iodoanisole. After it was separated, the free iodine was washed with 5% sodium sulfite, then washed with water, distilled under reduced pressure, and the fractions with a boiling point of 140-160 °C (5.33 kPa) were collected and cooled to 0 °C for filtration. Wash with methanol and recrystallize to obtain the finished product.Purification Methods
Crystallise 4-iodoanisole from aqueous EtOH and/or distil it under vacuum. [Beilstein 6 H 208, 6 I 109, 6 II 199, 6 III 744, 6 IV 1075.]4-아이오딘아니솔 준비 용품 및 원자재
원자재
준비 용품
4-알릴아니솔
Benzeneacetic acid, α-acetyl-4-methoxy-, ethyl ester
4-BROMO-4'-METHOXYBENZOPHENONE
Ethyl 4-methoxycinnamate
6-Methoxy-2-(4-methoxyphenyl)benzobithiophene
4,4'-DIMETHOXYDIPHENYLAMINE
(4-METHOXYPHENYLETHYNYL)TRIMETHYLSILANE&
4,4'-Dimethoxybiphenyl
1H-Benzimidazole,1-butyl-(9CI)
1-(4-METHOXYPHENYL)-1H-IMIDAZOLE
4-아이오딘아니솔 공급 업체
글로벌( 419)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| Hebei Mojin Biotechnology Co., Ltd | +8613288715578 |
sales@hbmojin.com | China | 12470 | 58 |
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 |
info@fdachem.com | China | 18223 | 58 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 |
info@dakenam.com | China | 15956 | 58 |
| Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 |
info@tianfuchem.com | China | 21689 | 55 |
| Hangzhou FandaChem Co.,Ltd. | 008657128800458; +8615858145714 |
fandachem@gmail.com | China | 9341 | 55 |
| career henan chemical co | +86-0371-86658258 |
sales@coreychem.com | China | 29914 | 58 |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 |
admin@nexconn.com | China | 10247 | 58 |
| Accela ChemBio Inc. | (+1)-858-699-3322 |
info@accelachem.com | United States | 19965 | 58 |
| Hebei Guanlang Biotechnology Co., Ltd. | +86-19930503282 |
alice@crovellbio.com | China | 8822 | 58 |
| Chongqing Chemdad Co., Ltd | +86-023-61398051 +8613650506873 |
sales@chemdad.com | China | 39916 | 58 |