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1-bromo-4-fluoro-2-(methoxy-d3)benzene

CAS No.
Chemical Name:
1-bromo-4-fluoro-2-(methoxy-d3)benzene
Synonyms
CBNumber:
CB68224776
Molecular Formula:
Molecular Weight:
0
MDL Number:
MOL File:
Mol file
Last updated:2023-10-18 10:04:29

1-bromo-4-fluoro-2-(methoxy-d3)benzene Chemical Properties,Uses,Production

Synthesis

2-Bromo-5-fluorophenol (1 g, 5.2 mmol), deuterated methyl iodide (911 mg, 6.3 mmol), and potassium carbonate (1.45 g, 10.5 mmol) were added to N, N-dimethylformamide (10 mL). The reaction solution was stirred and reacted for 6 h. After that, the reaction solution was cooled to room temperature. Ethyl acetate (20 mL) was added, and the reaction solution was washed with water (20 mL×3). The organic phases were combined, dried over anhydrous sodium sulfate, and filtered. The filtrate was concentrated under reduced pressure, and the resulting residue was purified by silica gel column chromatography with eluent system A to obtain 1-bromo-4-fluoro-2-(methoxy-d3)benzene. 1-bromo-4-fluoro-2-(methoxy-d3)benzene

1-bromo-4-fluoro-2-(methoxy-d3)benzene Preparation Products And Raw materials

Raw materials

Preparation Products

1-bromo-4-fluoro-2-(methoxy-d3)benzene Suppliers

Global( 1)Suppliers
Supplier Tel Email Country ProdList Advantage
Shanghai Boc Chemical Co., Ltd.
021-34975602; +8618721111801 shangli@bocchem.com China 138 58
Supplier Advantage
Shanghai Boc Chemical Co., Ltd.
58
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