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1-bromo-4-fluoro-2-(methoxy-d3)benzene

1-bromo-4-fluoro-2-(methoxy-d3)benzene Suppliers list
Company Name: Shanghai Boc Chemical Co., Ltd.
Tel: 021-34975602; +8618721111801
Email: shangli@bocchem.com
Products Intro: Product Name:1-bromo-4-fluoro-2-(methoxy-d3)benzene
Purity:0.98
1-bromo-4-fluoro-2-(methoxy-d3)benzene Basic information
Product Name:1-bromo-4-fluoro-2-(methoxy-d3)benzene
Synonyms:
CAS:
MF:
MW:0
EINECS:
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Mol File:Mol File
1-bromo-4-fluoro-2-(methoxy-d3)benzene Structure
1-bromo-4-fluoro-2-(methoxy-d3)benzene Chemical Properties
Safety Information
MSDS Information
1-bromo-4-fluoro-2-(methoxy-d3)benzene Usage And Synthesis
Synthesis2-Bromo-5-fluorophenol (1 g, 5.2 mmol), deuterated methyl iodide (911 mg, 6.3 mmol), and potassium carbonate (1.45 g, 10.5 mmol) were added to N, N-dimethylformamide (10 mL). The reaction solution was stirred and reacted for 6 h. After that, the reaction solution was cooled to room temperature. Ethyl acetate (20 mL) was added, and the reaction solution was washed with water (20 mL×3). The organic phases were combined, dried over anhydrous sodium sulfate, and filtered. The filtrate was concentrated under reduced pressure, and the resulting residue was purified by silica gel column chromatography with eluent system A to obtain 1-bromo-4-fluoro-2-(methoxy-d3)benzene. 1-bromo-4-fluoro-2-(methoxy-d3)benzene
1-bromo-4-fluoro-2-(methoxy-d3)benzene Preparation Products And Raw materials
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