1-(2-Bromoethyl)-4-(trifluoromethyl)benzene, 2-(4-Trifluoromethylphenyl)ethyl bromide
- CAS No.
- 130365-87-6
- Chemical Name:
- 1-(2-Bromoethyl)-4-(trifluoromethyl)benzene, 2-(4-Trifluoromethylphenyl)ethyl bromide
- Synonyms
- 4-TrifluoroMethylphenyl)ethyl broMide;4-(Trifluoromethyl)phenethyl bromide;2-(4-trifluoromethylphenyl)ethyl bromide;4-(TrifluoroMethyl)phenethyl broMide 97%;1-(2-broMoethyl)-4-(trifluoroMethyl)benzene;Benzene, 1-(2-bromoethyl)-4-(trifluoromethyl)-;1-(2-Bromoethyl)-4-(trifluoromethyl)benzene, 2-(4-Trifluoromethylphenyl)ethyl bromide
- CBNumber:
- CB82096863
- Molecular Formula:
- C9H8BrF3
- Molecular Weight:
- 253.06
- MDL Number:
- MFCD10567022
- MOL File:
- 130365-87-6.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Boiling point | 218.0±35.0 °C(Predicted) |
|---|---|
| Density | 1.499 g/mL at 25 °C |
| refractive index | n20/D 1.487 |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| form | liquid |
| Appearance | Colorless to light yellow Liquid |
| InChI | 1S/C9H8BrF3/c10-6-5-7-1-3-8(4-2-7)9(11,12)13/h1-4H,5-6H2 |
| InChIKey | WTCVMJLGKMOROW-UHFFFAOYSA-N |
| SMILES | FC(F)(F)c1ccc(CCBr)cc1 |
| Comptox DTXSID | DTXSID10565938 |
| UNSPSC Code | 12352100 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H319 |
| Precautionary statements | P264-P270-P280-P301+P312-P305+P351+P338-P337+P313 |
| PPE | Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter |
| Hazard Codes | Xn,N |
| Risk Statements | 22-36-51/53 |
| Safety Statements | 26-61 |
| RIDADR | UN 3082 9/PG 3 |
| WGK Germany | 3 |
| HS Code | 2903998090 |
| Storage Class | 10 - Combustible liquids |
| Hazard Classifications | Acute Tox. 4 Oral Eye Irrit. 2 |
1-(2-Bromoethyl)-4-(trifluoromethyl)benzene, 2-(4-Trifluoromethylphenyl)ethyl bromide price More Price(34)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 692050 | 4-(Trifluoromethyl)phenethyl bromide 97% | 130365-87-6 | 1g | $112 | 2026-04-30 | Buy |
| Apolloscientific | PC530024 | 4-Trifluoromethylphenethyl bromide 95% | 130365-87-6 | 250mg | $33 | 2026-06-04 | Buy |
| Apolloscientific | PC530024 | 4-Trifluoromethylphenethyl bromide 95% | 130365-87-6 | 1g | $49 | 2026-06-04 | Buy |
| Apolloscientific | PC530024 | 4-Trifluoromethylphenethyl bromide 95% | 130365-87-6 | 5g | $203 | 2026-06-04 | Buy |
| Apolloscientific | PC530024 | 4-Trifluoromethylphenethyl bromide 95% | 130365-87-6 | 25g | $893 | 2026-06-04 | Buy |
1-(2-Bromoethyl)-4-(trifluoromethyl)benzene, 2-(4-Trifluoromethylphenyl)ethyl bromide Chemical Properties, Uses, Production
Synthesis
2968-93-6
130365-87-6
Step ii: Synthesis of 1-(2-bromoethyl)-4-(trifluoromethyl)benzene To a 50 mL round bottom flask was added 2-(4-(trifluoromethyl)phenyl)ethanol (7.9 g, 0.0415 mol) and phosphorus tribromide (5.6 g, 0.0207 mol). The reaction mixture was stirred at 100 °C for 2 hours. After completion of the reaction, the reaction was quenched by adding ice-cold water to the mixture. The reaction mixture was extracted with hexane and the organic layer was separated. The organic layer was washed with brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure to give the crude product. The crude product was purified by column chromatography using 60-120 mesh silica gel as stationary phase and 0-5% ethyl acetate in hexane solution as eluent to give 4-(trifluoromethyl)phenylethyl bromide (7.8 g, 74% yield). 1H NMR (300 MHz, CDCl3): δ 7.60 (d, 2H), 7.35 (d, 2H), 3.61 (t, 2H), 3.25 (t, 2H).
References
[1] Patent: WO2015/101928, 2015, A1. Location in patent: Page/Page column 127;
[2] Patent: WO2005/123748, 2005, A1. Location in patent: Page/Page column 97-98
[3] Patent: WO2005/49613, 2005, A1. Location in patent: Page/Page column 48-49
[4] Patent: WO2007/69986, 2007, A1. Location in patent: Page/Page column 87
1-(2-Bromoethyl)-4-(trifluoromethyl)benzene, 2-(4-Trifluoromethylphenyl)ethyl bromide Preparation Products And Raw materials
1-(2-Bromoethyl)-4-(trifluoromethyl)benzene, 2-(4-Trifluoromethylphenyl)ethyl bromide Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Energy Chemical | 400-0056266 | sales8178@energy-chemical.com | China | 44567 | 61 |
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42917 | 64 |
| Syntechem Co.,Ltd | info@syntechem.com | China | 12973 | 57 | |
| Shanghai Litong Chemical Technology Co.,Ltd. | 13598610367 0373-7129549 | 2468833170@qq.com | China | 932 | 58 |
| Shanghai Topbiochem Technology Co., Ltd | 021-58170097 | info@topbiochem.com | China | 9509 | 58 |
| Amatek Scientific Co. Ltd. | 0512-56316828 4008675858 | sales@amateksci.com | China | 9848 | 55 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| Sigma-Aldrich | 021-61415566 800-8193336 | orderCN@merckgroup.com | China | 51389 | 80 |
| Zhengzhou Guancheng Laboratory equipment Sales | 0371-88888888 qq272369594;2159423853qq | 2723695949@qq.com | China | 4990 | 50 |
| Shanghai YuanYe Biotechnology Co., Ltd. | 18916372613 | yanzihan@shyuanye.com | China | 87240 | 60 |
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