4-Chlorobenzenesulfonyl chloride
- CAS No.
- 98-60-2
- Chemical Name:
- 4-Chlorobenzenesulfonyl chloride
- Synonyms
- 4-CHLOROBENZENE-1-SULFONYL CHLORIDE;CHLOROBENZENESULFONYL CHLORIDE;4-Chlorobenzene;4-Chlorobenzenesulfo;p-Chlorbenzensulfochlorid;p-Chlorobenzenesulfochloride;4-Chlorophenylchloro sulfone;p-Chlorobenzenesulfonylchlori;p-chlorophenylsulfonylchloride;4-chloro-benzenesulfonylchlorid
- CBNumber:
- CB8442402
- Molecular Formula:
- C6H4Cl2O2S
- Molecular Weight:
- 211.07
- MDL Number:
- MFCD00007439
- MOL File:
- 98-60-2.mol
- MSDS File:
- SDS
Melting point | 50-52 °C (lit.) |
---|---|
Boiling point | 141 °C/15 mmHg (lit.) |
Density | 1.5075 (estimate) |
Flash point | 226 °F |
storage temp. | under inert gas (nitrogen or Argon) at 2-8°C |
solubility | soluble in Toluene |
form | Liquid |
color | Clear |
Water Solubility | INSOLUBLE |
Sensitive | Moisture Sensitive |
BRN | 511583 |
CAS DataBase Reference | 98-60-2(CAS DataBase Reference) |
EWG's Food Scores | 1 |
FDA UNII | H55O3362D6 |
NIST Chemistry Reference | 4-Chlorobenzenesulfonyl chloride(98-60-2) |
EPA Substance Registry System | Benzenesulfonyl chloride, 4-chloro- (98-60-2) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS05 |
|||||||||
---|---|---|---|---|---|---|---|---|---|---|
Signal word | Danger | |||||||||
Hazard statements | H314 | |||||||||
Precautionary statements | P260-P280-P303+P361+P353-P304+P340+P310-P305+P351+P338-P363 | |||||||||
Hazard Codes | C | |||||||||
Risk Statements | 34-37 | |||||||||
Safety Statements | 26-28-36/37/39-45 | |||||||||
RIDADR | UN 3261 8/PG 2 | |||||||||
WGK Germany | 2 | |||||||||
RTECS | DB8925000 | |||||||||
F | 21 | |||||||||
Hazard Note | Corrosive | |||||||||
TSCA | Yes | |||||||||
HazardClass | 8 | |||||||||
PackingGroup | II | |||||||||
HS Code | 29049020 | |||||||||
NFPA 704 |
|
4-Chlorobenzenesulfonyl chloride price More Price(30)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich | 133698 | 4-Chlorobenzenesulfonyl chloride 97% | 98-60-2 | 5g | $36.4 | 2024-03-01 | Buy |
Sigma-Aldrich | 133698 | 4-Chlorobenzenesulfonyl chloride 97% | 98-60-2 | 100g | $138 | 2024-03-01 | Buy |
TCI Chemical | C0128 | 4-Chlorobenzenesulfonyl Chloride >98.0%(T) | 98-60-2 | 25g | $29 | 2024-03-01 | Buy |
TCI Chemical | C0128 | 4-Chlorobenzenesulfonyl Chloride >98.0%(T) | 98-60-2 | 500g | $137 | 2024-03-01 | Buy |
Sigma-Aldrich | 133698 | 4-Chlorobenzenesulfonyl chloride 97% | 98-60-2 | 500g | $229 | 2024-03-01 | Buy |
4-Chlorobenzenesulfonyl chloride Chemical Properties,Uses,Production
Chemical Properties
white to light yellow crystals, powder or flakes
Uses
4-Chlorobenzenesulfonyl chloride was used in the synthesis of precursors for the 3,4-pyridyne generation.
Production Methods
4-Chlorobenzenesulfonyl chloride is manufactured by mixing 4-chlorobenzene and chlorosulfuric acid at 35 ℃, heating for two hours at 80 ℃, and discharging the contents of the reactor into ice water; yield 81% of theory, together with a small amount of bis(4-chlorophenyl) sulfone.
Application
Used in the manufacture of chlorobenzenesulfinic acid and sulfimides; three-step reaction to the sulfone in a single reactor is possible without intermediate isolation.
Synthesis Reference(s)
The Journal of Organic Chemistry, 7, p. 15, 1942 DOI: 10.1021/jo01195a003
Purification Methods
Crystallise it from ether in powdered Dry-Ice, after the solution has been washed with 10% NaOH until colourless and dried (Na2SO4). Distil it in vacuo and store it in the absence of H2O. [Beilstein 11 IV 114.]
4-Chlorobenzenesulfonyl chloride Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
1of3
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 | info@fdachem.com | China | 20287 | 58 |
Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 | info@spring-chem.com | China | 2068 | 57 |
Capot Chemical Co.,Ltd. | +86-(0)57185586718 +86-13336195806 | sales@capot.com | China | 29791 | 60 |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18779 | 58 |
Shanghai Time Chemicals CO., Ltd. | +86-021-57951555 +8617317452075 | jack.li@time-chemicals.com | China | 1803 | 55 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29884 | 58 |
Hubei Jusheng Technology Co.,Ltd. | 18871490254 | linda@hubeijusheng.com | CHINA | 28172 | 58 |
Xiamen AmoyChem Co., Ltd | +86-86-5926051114 +8618959220845 | sales@amoychem.com | China | 6383 | 58 |
Hubei xin bonus chemical co. LTD | 86-13657291602 | linda@hubeijusheng.com | CHINA | 22963 | 58 |
Shandong chuangyingchemical Co., Ltd. | 18853181302 | sale@chuangyingchem.com | CHINA | 5906 | 58 |
View Lastest Price from 4-Chlorobenzenesulfonyl chloride manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2023-12-26 | 4-Chlorobenzenesulfonyl chloride
98-60-2
|
US $100.00-1.00 / KG | 1KG | 99% | g-kg-tons, free sample is available | Henan Fengda Chemical Co., Ltd | ||
2021-07-13 | 4-Chlorobenzenesulfonyl chloride
98-60-2
|
US $15.00-10.00 / KG | 1KG | 99%+ HPLC | Monthly supply of 1 ton | Zhuozhou Wenxi import and Export Co., Ltd | ||
2019-11-08 | 4-Chlorobenzenesulfonyl chloride
98-60-2
|
US $0.00 / g | 1g | 98%min | 20kg/month | Nanjing jinheyou Trading Co., Ltd. |
- 4-Chlorobenzenesulfonyl chloride
98-60-2
- US $100.00-1.00 / KG
- 99%
- Henan Fengda Chemical Co., Ltd
- 4-Chlorobenzenesulfonyl chloride
98-60-2
- US $15.00-10.00 / KG
- 99%+ HPLC
- Zhuozhou Wenxi import and Export Co., Ltd
- 4-Chlorobenzenesulfonyl chloride
98-60-2
- US $0.00 / g
- 98%min
- Nanjing jinheyou Trading Co., Ltd.