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Protoporphyrin IX dimethyl ester

CAS No.
5522-66-7
Chemical Name:
Protoporphyrin IX dimethyl ester
Synonyms
Protoporphyrin dimethyl;dimethyl protoporphyrin IX;Protoporphyrin IX diMethyl es;Protoporphyrin IX dimethyl ester;Dimethylprotoporphyrin IX dimethyl ester;Protoporphyrin IX dimethyl ester, ≥95%(HPLC);Protoporphyrin IX dimethyl ester ~90% (HPLC);PROTOPORPHYRIN IX DIMETHYL ESTER FROM*OX HEMIN;dimethyl 8,13-divinyl-3,7,12,17-tetramethyl-21h,23h-porphine-2,18-dipropionate;dimethyl 3,8,13,17-tetramethyl-7,12-divinyl-21H,23H-porphine-2,18-dipropionate
CBNumber:
CB9497515
Molecular Formula:
C36H38N4O4
Molecular Weight:
590.71
MDL Number:
MFCD29047709
MOL File:
5522-66-7.mol
MSDS File:
SDS
Last updated:2024-11-25 20:05:57

Protoporphyrin IX dimethyl ester Properties

Melting point 225-228 °C(lit.)
Boiling point 1017.0±65.0 °C(Predicted)
Density 1.220±0.06 g/cm3(Predicted)
storage temp. Keep in dark place,Inert atmosphere,2-8°C
solubility DMSO: soluble
form crystal
color purple
BRN 381574
Stability Light Sensitive
FDA UNII PHV7RHT9L3
EPA Substance Registry System 21H,23H-Porphine-2,18-dipropanoic acid, 7,12-diethenyl-3,8,13,17-tetramethyl-, dimethyl ester (5522-66-7)

SAFETY

Risk and Safety Statements

WGK Germany  3
8-10-23

Protoporphyrin IX dimethyl ester price More Price(9)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 09626 Protoporphyrin IX dimethyl ester ~90% (HPLC) 5522-66-7 100mg $190 2024-03-01 Buy
Strem Chemicals 07-1850 Protoporphyrin IX, dimethyl ester 5522-66-7 100mg $87 2024-03-01 Buy
Strem Chemicals 07-1850 Protoporphyrin IX, dimethyl ester 5522-66-7 500mg $308 2024-03-01 Buy
TRC P838900 Protoporphyrin IX dimethyl ester 5522-66-7 1g $425 2021-12-16 Buy
TRC P838900 Protoporphyrin IX dimethyl ester 5522-66-7 100mg $65 2021-12-16 Buy
Product number Packaging Price Buy
09626 100mg $190 Buy
07-1850 100mg $87 Buy
07-1850 500mg $308 Buy
P838900 1g $425 Buy
P838900 100mg $65 Buy

Protoporphyrin IX dimethyl ester Chemical Properties,Uses,Production

Uses

Protoporphyrin IX Dimethyl Ester is a derivative of Protoporphyrin IX (P839138), which is an important precursor to biologically essential prosthetic groups such as heme, cytochrome c, and chlorophylls.

Definition

ChEBI: Dimethylprotoporphyrin IX dimethyl ester is a member of porphyrins.

Purification Methods

The crude dimethyl ester (1g) in CHCl3 (200 mL) is mixed with pet ether (b 70-90o, 600mL), and any porphyrin (m > 260o) which is insoluble in this mixture is filtered off. The filtrate is passed through a column of CaCO3 [from CaCO3 (130g) which is kept overnight in a mixture of CHCl3/pet ether (b 70-90o, 1:3), and the slurry is poured into a glass tube (2.5 x 26cm) to form the column]. After all the filtrate is applied, the column is eluted with a solution of CHCl3/pet ether (b 70-90o, 1:3). All the coloured eluates are collected, evaporated at room temperature in a vacuum to give a residue (0.8g), m 208-211o. The residue (0.8g) in CHCl3 (66mL) is heated briefly to its boiling point, then boiling MeOH (198mL) is added immediately to it. The mixture is allowed to cool to room temperature, refrigerated for 2days and the solid is filtered off. The solid is washed on the filter funnel with CHCl3/MeOH (1:9, 50mL) and dried at 50o/vacuum (yield 0.62-0.66g). It can also be recrystallised by dissolving in as little hot dry *C6H6 as possible and left overnight at 20o, m 228-230o. It has also been purified by dissolving (0.4g) in CHCl3 (33mL) by boiling for a few minutes, then diluting with boiling MeOH (100mL) and refrigerating for 2days. The crystals are collected, washed with CHCl3/MeOH (1:9) and dried at 50o in a vacuum (yield 0.3g). The UV has max at 631, 576, 541, 506 and 407nm in CHCl3 and 601, 556 and 406nm in 25% HCl. [Ramsey Biochemical Preparations 3 39 1953, Beilstein 26 III/IV 3052.]

553-12-8
5522-66-7
Synthesis of Protoporphyrin IX dimethyl ester from Protoporphyrin IX
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View Lastest Price from Protoporphyrin IX dimethyl ester manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
Protoporphyrin IX dimethyl ester pictures 2024-11-25 Protoporphyrin IX dimethyl ester
5522-66-7
US $10.00 / KG 100KG 99% 100 mt Hebei Weibang Biotechnology Co., Ltd
Protoporphyrin IX dimethyl ester pictures 2024-11-18 Protoporphyrin IX dimethyl ester
5522-66-7
US $0.00-0.00 / KG 1KG 95.0% 10000KGS Shaanxi Dideu New Materials Co. Ltd
Protoporphyrin IX dimethyl ester pictures 2024-10-11 Protoporphyrin IX dimethyl ester
5522-66-7
US $1.90 / KG 1KG 99% 10 ton Hebei Chuanghai Biotechnology Co,.LTD
methyl 3-[8,13-di(ethenyl)-18-(3-methoxy-3-oxo-propyl)-3,7,12,17-tetramethyl-22,23-dihydroporphyrin-2-yl]propanoate methyl 3-[8,13-di(ethenyl)-18-(3-methoxy-3-oxopropyl)-3,7,12,17-tetramethyl-22,23-dihydroporphyrin-2-yl]propanoate Protoporphyrin IX diMethyl es 21H,23H-Porphine-2,18-dipropanoicacid, 7,12-diethenyl-3,8,13,17-tetraMethyl-, 2,18-diMethyl ester ProtoporphyrinIX dimethyl ester,Dimethyl 8,13-divinyl-3,7,12,17-tetramethyl-21H,23H-porphine-2,18-dipropionate, Ooporpyhrin dimethyl ester dimethyl 8,13-divinyl-3,7,12,17-tetramethyl-21h,23h-porphine-2,18-dipropionate 7,12-diethenyl-3,8,13,17-tetramethyl-21H,23H-Porphine-2,18-dipropanoic acid- 2,18-dimethyl ester Dimethylprotoporphyrin IX dimethyl ester dimethyl protoporphyrin IX Ooporpyhrin dimethyl ester, Dimethyl 8,13-divinyl-3,7,12,17-tetramethyl-21H,23H-porphine-2,18-dipropionate 3,8,13,17-Tetramethyl-7,12-diethenyl-21H,23H-porphyrin-2,18-dipropionic acid dimethyl ester 7,12-Diethenyl-3,8,13,17-tetramethyl-21H,23H-porphyrin-2,18-bis(propionic acid methyl) ester Protoporphyrin dimethyl 3-[18-(3-keto-3-methoxy-propyl)-3,7,12,17-tetramethyl-8,13-divinyl-22,23-dihydroporphin-2-yl]propionic acid methyl ester dimethyl 3,8,13,17-tetramethyl-7,12-divinyl-21H,23H-porphine-2,18-dipropionate PROTOPORPHYRIN IX DIMETHYL ESTER FROM*OX HEMIN Protoporphyrin IX dimethyl ester Protoporphyrin IX dimethyl ester, ≥95%(HPLC) Protoporphyrin IX dimethyl ester ~90% (HPLC) Dimethyl 3,3'-(3,8,13,17-tetramethyl-7,12-divinylporphyrin-2,18-diyl)dipropionate 2,18-Dimethyl 7,12-diethenyl-3,8,13,17-tetramethyl-21H,23H-porphine-2,18-dipropanoate Dimethyl 3,3'-(3,8,13,17-tetramethyl-7,12-divinylporphyrin-2,18-diyl)dipropionate 5522-66-7 porphine (porphyrin) ligand