1-Bromo-2-(2-methoxyethoxy)ethane

- CAS No.
- 54149-17-6
- Chemical Name:
- 1-Bromo-2-(2-methoxyethoxy)ethane
- Synonyms
- DK815;DKSI138;mPEG2-Br;DKFELEX0212;CAS_54149-17-6;Bromo-PEG2-methoxy;Methyl-PEG2-bromide;1-bromo-3,6-dioxaheptane;MONO METHOXY PEG BROMIDE;1-BROMO-(2-METHOXYETHOXY)ETHANE
- CBNumber:
- CB2216300
- Molecular Formula:
- C5H11BrO2
- Molecular Weight:
- 183.04
- MOL File:
- 54149-17-6.mol
- MSDS File:
- SDS
- Modify Date:
- 2025/4/17 18:22:24
Boiling point | 156 °C (lit.) 37-40 °C/0.01 mmHg (lit.) |
---|---|
Density | 1.3600 g/mL at 25 °C (lit.) |
refractive index |
n |
Flash point | 163 °F |
storage temp. | 2-8°C |
form | Liquid |
color | Clear colorless to pale yellow |
Water Solubility | Not miscible in water. |
Sensitive | Light Sensitive |
BRN | 2069579 |
InChI | InChI=1S/C5H11BrO2/c1-7-4-5-8-3-2-6/h2-5H2,1H3 |
InChIKey | HUXJXNSHCKHFIL-UHFFFAOYSA-N |
SMILES | C(OCCBr)COC |
CAS DataBase Reference | 54149-17-6(CAS DataBase Reference) |
NIST Chemistry Reference | 1-Bromo-2-(2-methoxyethoxy)ethane(54149-17-6) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS07 |
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Signal word | Warning | |||||||||
Hazard statements | H227 | |||||||||
Precautionary statements | P210e-P280a-P370+P378a-P403+P235-P501a | |||||||||
Risk Statements | 36/37/38 | |||||||||
Safety Statements | 24/25 | |||||||||
WGK Germany | 3 | |||||||||
HS Code | 29091990 | |||||||||
NFPA 704 |
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1-Bromo-2-(2-methoxyethoxy)ethane price More Price(7)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich(India) | 639842 | 1-Bromo-2-(2-methoxyethoxy)ethane 95% | 54149-17-6 | 10G | ₹16464.83 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | 639842 | 1-Bromo-2-(2-methoxyethoxy)ethane 95% | 54149-17-6 | 50G | ₹65253.1 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | 456195 | 1-Bromo-2-(2-methoxyethoxy)ethane 90% | 54149-17-6 | 10G | ₹9650 | 2022-06-14 | Buy |
ALFA India | ALF-L05406-14 | 1-Bromo-2-(2-methoxyethoxy)ethane, tech. 90%, stab. with sodium carbonate | 54149-17-6 | 25g | ₹15713 | 2022-05-26 | Buy |
ALFA India | ALF-L05406-06 | 1-Bromo-2-(2-methoxyethoxy)ethane, tech. 90%, stab. with sodium carbonate | 54149-17-6 | 5g | ₹4773 | 2022-05-26 | Buy |
1-Bromo-2-(2-methoxyethoxy)ethane Chemical Properties,Uses,Production
Chemical Properties
clear colorless to pale yellow liquid
Uses
1-Bromo-2-(2-methoxyethoxy)ethane is an important raw material and intermediate used in organic synthesis, pharmaceuticals, agrochemicals and dyestuff.
Synthesis
General Procedure for Preparation of 1-Bromo-2-(2-methoxyethoxy)ethane: Into a 25-mL round bottomed flask equipped with magnetic stir bar, addition funnel and positive flow of nitrogen were placed 15.60 mmol of a ethyleneglycol monomethyl ether. The solution was stirred for 15 min in an ice bath before the dropwise addition of phosphorous tribromide (7.81 mmol) over a 10 min period. The solution was allowed to gradually warm and stir at room temperature (rt) for 14 hrs. The solution was then heated in a 90 °C oil bath for 1 hr, at which time the solution turned yellow. The solution was allowed to cool to rt, poured onto 30 g of ice/water mixture, and made slightly basic with addition of a 10% solution of NaHCO3 (~6 mL). Subsequent extraction with diethyl ether (Et2O) (3 x 30 mL), followed by drying over MgSO4 and concentration under reduced pressure afforded a colorless oil in sufficient purity for use in subsequent reactions.
1-Bromo-2-(2-methoxyethoxy)ethane Preparation Products And Raw materials
Supplier | Tel | Country | ProdList | Advantage | Inquiry |
---|---|---|---|---|---|
SynthoCascade Research Laboratories | +91-9440962500 +91-9440962500 | Telangana, India | 284 | 58 | Inquiry |
CHEMSWORTH | +91-261-2397244 | New Delhi, India | 6700 | 30 | Inquiry |
TCI Chemicals (India) Pvt. Ltd. | 1800 425 7889 | New Delhi, India | 6768 | 58 | Inquiry |
Alfa Aesar | 1 800 209 7001 | Maharashtra, India | 6905 | 58 | Inquiry |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-+86-371-66670886 | China | 19809 | 58 | Inquiry |
Shanghai Zhuangming Biopharma Co., Ltd. | +86-19189228086 +86-18858568638 | China | 641 | 58 | Inquiry |
Hebei Xinsheng New Material Technology Co., LTD. | +86-16632316109 | China | 1085 | 58 | Inquiry |
Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | China | 21628 | 55 | Inquiry |
Accela ChemBio Inc. | +1-858-6993322 | United States | 19825 | 58 | Inquiry |
Changzhou Ditong Chemical Co.,Ltd | +86-0519-88299272 | China | 2176 | 58 | Inquiry |
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