N,N'-BIS(2-HYDROXYETHYL)-UREA

N,N'-BIS(2-HYDROXYETHYL)-UREA Structure
CAS No.
15438-70-7
Chemical Name:
N,N'-BIS(2-HYDROXYETHYL)-UREA
Synonyms
Nsc 75436;Diethylolurea;Diethanolurea;NN'-Diethanolurea;2,2'-Ureylenediethanol;2,2'-(Ureylene)diethanol;1,3-Bis(2-hydroxyethyl)urea;N,N'-Di-(2-hydroxyethyl)urea;N,N'-BIS(2-HYDROXYETHYL)UREA;1,3-Di(beta-hydroxyethyl)urea
CBNumber:
CB3227802
Molecular Formula:
C5H12N2O3
Molecular Weight:
148.16
MOL File:
15438-70-7.mol
MSDS File:
SDS
Modify Date:
2023/4/23 13:52:06

N,N'-BIS(2-HYDROXYETHYL)-UREA Properties

Melting point 83 °C
Boiling point 445.1±30.0 °C(Predicted)
Density 1.226±0.06 g/cm3(Predicted)
storage temp. -20°C Freezer, Under inert atmosphere
solubility DMSO (Slightly)
form Solid
pka 13.09±0.46(Predicted)
color Off-White to Light Beige
EPA Substance Registry System Urea, N,N'-bis(2-hydroxyethyl)- (15438-70-7)

SAFETY

Risk and Safety Statements

N,N'-BIS(2-HYDROXYETHYL)-UREA Chemical Properties,Uses,Production

Preparation

Excess ethanolamine and DMDTC were mixed and heated at 60℃ for 15 h. The released malodorous methyl sulfide by-product was absorbed and oxidized by NaOCl solution. When the reaction was complete, the unreacted ethanolamine was removed under reduced pressure by simple distillation, leaving a crude mixture of oxazolidinone and bis(2-hydroxyethyl)urea, which was further purified by recrystallization from methanol/ethyl acetate (1:4.5) to give N,N'-bis(2-hydroxyethyl)urea as colorless crystals.

N,N'-BIS(2-HYDROXYETHYL)-UREA Preparation Products And Raw materials

Raw materials

Preparation Products

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N,N'-BIS(2-HYDROXYETHYL)-UREA 1,3-Bis(2-hydroxyethyl)urea 2,2'-(Ureylene)diethanol 2,2'-Ureylenediethanol 1,3-Di(beta-hydroxyethyl)urea Nsc 75436 Urea, 1,3-bis(2-hydroxyethyl)- (8ci) Urea, N,N'-bis(2-hydroxyethyl)- N,N'-Di-(2-hydroxyethyl)urea Diethanolurea Diethylolurea NN'-Diethanolurea N,N'-BIS(2-HYDROXYETHYL)UREA 15438-70-7