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tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate

	tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate Structure
CAS No.
173405-78-2
Chemical Name:
tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate
Synonyms
TERT-BUTYL 3,9-DIAZASPIRO[5.5]UNDECANE-3-CARBOXYLATE;3-Boc-3,9-diazaspiro[5.5]...;3-Boc-3,9-Diazaspiro[5.5]undecane;3-N-Boc-3,9-diazaspiro[5.5]undecane;3-Boc-3,9-diazaspiro[5.5]undecane heMioxalate;Tert-Butyl3,9-Diazaspiro[5.5]Undecane-3-Carboxyla;tert-Butyl 3,9-diazaspiro5.5undecan-3-carboxylate;3,9-DIAZASPIRO[5.5]UNDECANE-3-CARBOXYLIC ACID T-BUTYL ESTER;1,1-Dimethylethyl 3,9-diazaspiro[5.5]undecane-3-carboxylate;3,9-DIAZA-SPIRO[5.5]UNDECANE-3-CARBOXYLIC ACID TERT-BUTYL ESTER
CBNumber:
CB5434952
Molecular Formula:
C14H26N2O2
Molecular Weight:
254.37
MOL File:
173405-78-2.mol
MSDS File:
SDS
Modify Date:
2023/12/18 13:44:43

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate Properties

Melting point 0°C
Boiling point 0°C
Density 1.05
Flash point 0°C
storage temp. 2-8°C(protect from light)
form solid
pka 11.00±0.20(Predicted)
color White

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P280-P305+P351+P338-P304+P340
Risk Statements  36/37/38-20/21/22-68
Safety Statements  26-36-36/37/39-28
HS Code  29339900

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate Chemical Properties,Uses,Production

Synthesis

Under argon atmosphere, wet Pd/C (188.05 mg, 159.50 μmol, purity 10%) was added into tert-butyl 9-benzyl-3,9-diazaspiro[5.5]undecane-3-carboxylate in THF solution (1.10 g, 3.19 mmol), after replacing the gas in the flask 3 times with hydrogen, the reaction was stirred at 40°C for 40 hours under 45 Psi. After completion of the reaction, the solution was filtered through diatomite. The filtrate was concentrated to give the crude tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate.
	tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate Spectrum

3,9-DIAZASPIRO[5.5]UNDECANE-3-CARBOXYLIC ACID T-BUTYL ESTER 3,9-DIAZA-SPIRO[5.5]UNDECANE-3-CARBOXYLIC ACID TERT-BUTYL ESTER Tert-Butyl3,9-Diazaspiro[5.5]Undecane-3-Carboxyla 3,9-Diazaspiro[5.5]undecane-3-carboxylic acid, 1,1-dimethylethyl ester 3-Boc-3,9-Diazaspiro[5.5]undecane 3-N-Boc-3,9-diazaspiro[5.5]undecane 3-Boc-3,9-diazaspiro[5.5]... 3,9-diaza-spiro[5.5]undecane-3-carboxylic acid tert-butyl ester hydrochloride 3,9-Diaza-spiro[5.5]undecane-3-carboxylic acid tert-butyl ester.HCl 3,9-Diazaspiro[5.5]undecane-3-acetic acid 1,1-diMethylethyl ester 3,9-Diazaspiro[5.5]undecane-3-carboxylic acid tert-butyl ester,95+ 3-Boc-3,9-diazaspiro[5.5]undecane heMioxalate 3,9-Diaza-Spiro[5.5]Undecane-3-Carboxylic Acid Tert-Butyl Es... TERT-BUTYL 3,9-DIAZASPIRO[5.5]UNDECANE-3-CARBOXYLATE 1,1-Dimethylethyl 3,9-diazaspiro[5.5]undecane-3-carboxylate tert-Butyl 3,9-diazaspiro5.5undecan-3-carboxylate 1,1-Dimethylethyl 9-acetyl-3,9-diazaspiro[5.5]undecane-3-carboxylate 173405-78-2 Heterocycles series pharmacetical