2-(2-chlorophenyl)cyclohexanone
- CAS No.
- 91393-49-6
- Chemical Name:
- 2-(2-chlorophenyl)cyclohexanone
- Synonyms
- 2-(2-chlorophenyl)cyclohexan-1-one;(2-chlorophenyl)cyclohexanone;2-(2-chlorophenyl)cyclohexanone;2-(2-Chlor-phenyl)-cyclohexanon;Cyclohexanone, 2-(2-chlorophenyl)-;2-(2-chlorophenyl)cyclohexanone liquid
- CBNumber:
- CB62756163
- Molecular Formula:
- C12H13ClO
- Molecular Weight:
- 208.68
- MOL File:
- 91393-49-6.mol
- Modify Date:
- 2024/7/23 11:51:51
| Melting point | 60-62 °C |
|---|---|
| Boiling point | 308.8±42.0 °C(Predicted) |
| Density | 1.165±0.06 g/cm3(Predicted) |
| form | powder |
| color | white crystalline |
| InChI | InChI=1S/C12H13ClO/c13-11-7-3-1-5-9(11)10-6-2-4-8-12(10)14/h1,3,5,7,10H,2,4,6,8H2 |
| InChIKey | UOEXWLLNMGAJDD-UHFFFAOYSA-N |
| SMILES | C1(=O)CCCCC1C1=CC=CC=C1Cl |
2-(2-chlorophenyl)cyclohexanone Chemical Properties,Uses,Production
Chemical Properties
white crystalline powder.
Uses
2-(2-Chlorophenyl)-cyclohexanone is a reactant that is used in the preparation of benzofurans via palladium-phosphine-catalyzed intramolecular enolate O-arylation of α-arylketones.
Synthesis
To a flame dried flask was added Cs2CO3 (6.5 g, 20 mmol), Pd2(dba)3 (184 mg, 0.2 mmol) and Xantphos (139 mmol, 0.24 mmol). After purging with N2, toluene (10 mL), ketone (15 mmol) and phenyl iodide (1.11 mL, 10 mmol) were added. After stirring overnight at 80 .MALE.C, the mixture was filtered and concentrated in vacuo to afford a residue, which was purified by flash chromatography to provide the desired 2-(2-chlorophenyl)cyclohexanone.
2-(2-chlorophenyl)cyclohexanone Preparation Products And Raw materials
Raw materials
Preparation Products
2-(2-chlorophenyl)cyclohexanone Suppliers
Global( 85)Suppliers
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|---|---|---|---|---|---|
| CLEARSYNTH LABS LTD. | +91-22-45045900 | Hyderabad, India | 6351 | 58 | Inquiry |
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| Hebei Xinsheng New Material Technology Co., LTD. | +86-16632316109 | China | 1090 | 58 | Inquiry |
2-(2-chlorophenyl)cyclohexanone
Cyclohexanone, 2-(2-chlorophenyl)-
(2-chlorophenyl)cyclohexanone
2-(2-Chlor-phenyl)-cyclohexanon
2-(2-chlorophenyl)cyclohexan-1-one
2-(2-chlorophenyl)cyclohexanone liquid
91393-49-6
intermediates
91393-49-6
Pharm