2-CHLORO-5-NITROBENZENESULFONIC ACID
![2-CHLORO-5-NITROBENZENESULFONIC ACID Structure](CAS/GIF/96-73-1.gif)
- CAS No.
- 96-73-1
- Chemical Name:
- 2-CHLORO-5-NITROBENZENESULFONIC ACID
- Synonyms
- NSC 5375;3-Sulfo-4-chloronitrobenzene;2-CHLORO-5-NITROSULFOBENZENE;2-chloro-5-nitro-benzenesulfonicaci;4-NITROCHLOROBENZENE-2-SULFONIC ACID;2-CHLORO-5-NITROBENZENESULFONIC ACID;P-NITROCHLOROBENZENE-O-SULFONIC ACID;2-Chloro-5-nitrobenzenesulfonec acid;2-CHLORO-5-NITROBENZENESULPHONIC ACID;1-Chloro-4-nitrobenzene-2-sulfonic Acid
- CBNumber:
- CB7113158
- Molecular Formula:
- C6H4ClNO5S
- Molecular Weight:
- 237.62
- MOL File:
- 96-73-1.mol
- Modify Date:
- 2023/10/21 10:37:28
Melting point | >300°C |
---|---|
Density | 1.651 (estimate) |
refractive index | 1.6000 (estimate) |
storage temp. | Refrigerator |
pka | -1.73±0.33(Predicted) |
form | solid |
CAS DataBase Reference | 96-73-1(CAS DataBase Reference) |
EPA Substance Registry System | Benzenesulfonic acid, 2-chloro-5-nitro- (96-73-1) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H317-H319 |
Precautionary statements | P280-P305+P351+P338 |
2-CHLORO-5-NITROBENZENESULFONIC ACID Chemical Properties,Uses,Production
Chemical Properties
Tan Solid
Physical properties
2-Chloro-5-nitrobenzenesulfonic Acid, crystallizes as the dihydrate from water (mp 169 ℃, decomp.). The compound undergoes explosive decomposition when heated above 200 ℃, and all reactions, including its production, must be undertaken with great caution.
Uses
Amination of 2-Chloro-5-nitrobenzenesulfonic Acid gives 4-nitroaniline- 2-sulfonic acid [96-75-3], which is used as a diazo component or reduced to the important colorant intermediate 2,5-diaminobenzenesulfonic acid [88-45-9]. Chlorination of 2-Chloro-5-nitrobenzenesulfonic Acid in aqueous solution is a more facile route to 2,6- dichloro-4-nitroaniline than chlorination of 4-nitroaniline.
Production Methods
4-Chloronitrobenzene is sulfonated with 65 % oleum at 115 ℃; special precaution must be taken to control temperature. Work-up is by quenching and isolation of the sodium salt after it has been salted out.
2-CHLORO-5-NITROBENZENESULFONIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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