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1,1-diethoxyethylene

1,1-diethoxyethylene Structure
CAS No.
2678-54-8
Chemical Name:
1,1-diethoxyethylene
Synonyms
KETENE DIETHYL ACETAL;1,1-DIETHOXYETHENE;Ethene, 1,1-diethoxy-;135338;1,1-Diethoxyethen;1,1-diethoxyethylene;Diethyl ketene acetal;1,1-Diethoxyethene, stabilized;2-(1-ethoxypropoxy)ethen-1-one;KETENE DIETHYL ACETAL STAB. WACKER &
CBNumber:
CB7429938
Molecular Formula:
C6H12O2
Molecular Weight:
116.16
MOL File:
2678-54-8.mol
MSDS File:
SDS
Modify Date:
2023/5/4 15:14:25

1,1-diethoxyethylene Properties

Boiling point 49-50 °C(lit.)
Density 0.880 g/mL at 20 °C(lit.)
refractive index n20/D 1.414
Flash point 27 °C
storage temp. 2-8°C

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS02
Signal word  Warning
Hazard statements  H226
Risk Statements  10
Safety Statements  23
RIDADR  UN 1993 3/PG 3
WGK Germany  3

1,1-diethoxyethylene Chemical Properties,Uses,Production

Uses

1,1-diethoxyethylene can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis

Synthesis_2678-54-8
Preparation of 1,1-diethoxyethene 610.4 g (4.0 mol) of chloroacetaldehyde diethyl acetal, 800 g (12.0 mol) of powdered technical grade potassium hydroxide, 32 g of polyethylene glycol 1000 dimethyl ether and 88 g (1.0 mol) of 2-methyl-2-butanol were heated to reflux in 1.2 l of tert.-butyl methyl ether while stirring. After six hours the reaction was stopped, the salts filtered off and the reaction mixture distilled at reduced pressure (5 kPa). 326 g (72.5% of theoretical) of 1,1-diethoxyethene (b.p. 49?? C./5 kPa) were obtained.

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Diethyl ketene acetal 1,1-Diethoxyethen KETENE DIETHYL ACETAL STAB. WACKER & 1,1-diethoxyethylene 2-(1-ethoxypropoxy)ethen-1-one 1,1-Diethoxyethene, stabilized 135338 KETENE DIETHYL ACETAL 1,1-DIETHOXYETHENE Ethene, 1,1-diethoxy- 1,1-diethoxyethene CAS NO.2678-54-8 CAS NO.2678-54-8 2678-54-8 Building Blocks Acetals/Ketals/Ortho Esters Organic Building Blocks Oxygen Compounds