2-(4-(tert-butyl)naphthalen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- CAS No.
- 2217657-10-6
- Chemical Name:
- 2-(4-(tert-butyl)naphthalen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- Synonyms
- 4-(tert-Butyl)naphthalene-2-boronic Acid Pinacol Ester;2-[4-(1,1-Dimethylethyl)-2-naphthalenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;1,3,2-Dioxaborolane, 2-[4-(1,1-dimethylethyl)-2-naphthalenyl]-4,4,5,5-tetramethyl-;2-[6-[3-(1,1-dimethylethyl)-4-methoxyphenyl]-2-naphthalenyl]-4,4,5,5-tetramethyl-1,3,2-Dioxaborolane
- CBNumber:
- CB78371918
- Molecular Formula:
- C20H27BO2
- Molecular Weight:
- 310.24
- MOL File:
- 2217657-10-6.mol
- Modify Date:
- 2024/6/13 17:47:58
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P280-P301+P312-P302+P352-P305+P351+P338 |
2-(4-(tert-butyl)naphthalen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane Chemical Properties,Uses,Production
Uses
2-(4-(tert-butyl)naphthalen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane is the key intermediate for the synthesis of OLED red dopant materials has been widely concerned and studied in recent years.
Preparation
The synthesis proceeded as follows: Successively, 600g of xylene (99%), 68.3g of intermediate B (0.2mol, 99.9%), 153.9g of biboronic acid pinacol ester (0.6mol, 99%), 1.5g of palladium acetate (0.01mol, 99%), and 16.6g of sodium acetate (0.2mol, 99%) were added. The mixture was heated to 110°C for 12 h, after which it was cooled to room temperature. The reaction mixture was then washed with water and the organic layer was dried over anhydrous sodium sulfate. Subsequently, xylene was evaporated to obtain the crude product. The crude product was recrystallized with ethyl acetate, resulting in the formation of 2-(4-(tert-butyl)naphthalen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane.
2-(4-(tert-butyl)naphthalen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane Preparation Products And Raw materials
Raw materials
Preparation Products
2-(4-(tert-butyl)naphthalen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane Suppliers
| Supplier | Tel | Country | ProdList | Advantage | Inquiry |
|---|---|---|---|---|---|
| Jiangsu Nata Opto-electronic Material Co.,Ltd. | +86-0512-62520998 +86-15030927757 | China | 229 | 58 | Inquiry |
| Coresyn Pharmatech Co., Ltd. | +86-571-86626709 +86-18157142896 | China | 9991 | 58 | Inquiry |
| Baynoe Chem (Suzhou) Co., Ltd. | +86-512 65869404 +86-18934593683 | China | 257 | 58 | Inquiry |
| Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 | China | 29798 | 60 | Inquiry |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | China | 10311 | 58 | Inquiry |
| QINGDAO KAIENSI INTERNATIONAL TRADE CO.,LTD. | +86-0532-8699-9256 +8615254267723 | China | 1410 | 58 | Inquiry |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | China | 14351 | 58 | Inquiry |
| ANHUI WITOP BIOTECH CO., LTD | +8615255079626 | China | 23555 | 58 | Inquiry |
| Yurui (Shanghai) Chemical Co., Ltd. | +86-021-50456736 +8615000292053 | China | 1031 | 58 | Inquiry |
| Hangzhou MolCore BioPharmatech Co.,Ltd. | +86-057181025280; +8617767106207 | China | 49739 | 58 | Inquiry |