2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate

CAS No.: 1041026-71-4

Chemical Name:: 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate

Synonyms: tert-butyl 2,6-diazaspiro[3.3]heptane-2-carboxylate oxalate;tert-Butyl 2,6-diazaspiro[3.3]heptane-2-carboxylate oxalate(2:1);2-Boc-2,6-diazaspiro[3.3]heptane Hemioxalate;6-diazaspiro[3.3]heptane-2-carboxylate oxalate;1-Boc-2,6-diazaspiro[3.3]heptanehemioxalate,97%;1-Boc-2,6-diazaspiro[3.3]heptane heMioxalate, 97%;2-Boc-2,6-Diazaspiro[3.3]heptane ethanedioate (2:1);2,6-Diazaspiro[3.3]heptane, N2-BOC protected hemioxalate;ert-Butyl 2,6-diazaspiro[3,3]heptane-2-carboxylate hemioxalate;tert-Butyl 2,6-diazaspiro[3,3]heptane-2-carboxylate hemioxalate

CBNumber:: CB82548539

Molecular Formula:: C22H38N4O8

Molecular Weight:: 486.56

MOL File:: 1041026-71-4.mol

Modify Date:: 2023/4/23 13:52:06

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2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate Properties

Melting point	206-209℃
storage temp.	under inert gas (nitrogen or Argon) at 2-8°C
solubility	DMSO (Slightly, Heated), Methanol (Slightly, Sonicated)
form	Solid
color	White to Off-White
Water Solubility	Slightly soluble in water.
Stability	Hygroscopic

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H302-H312

Precautionary statements

P264-P270-P280h-P301+P312a-P321-P501a

HS Code

2933399990

NFPA 704

	1
2		0

2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate Chemical Properties,Uses,Production

Chemical Properties

white to yellow Solid.

Uses

It is employed as a intermediate for pharmaceutical.

Preparation

Synthesis of 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate: Take a 500mL single-necked bottle, add 6-toluenesulfonyl-2,6-diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester (7g, 20mmol), dissolve in methanol (200mL), add magnesium chips (3.84 g) g, 0.16 mol, 8 equiv) and stirred at room temperature. The reaction solution gradually turned into a white viscous state with the dissolution of the magnesium scraps, and TLC showed that the reaction of the raw materials was completed. The solvent was removed by rotary evaporation, ether (150 mL) was added, stirred at room temperature for 1 h, filtered through celite, the filtrate was dried over anhydrous sodium sulfate, and an ethanol solution (3 mL) of anhydrous oxalic acid (0.89 g, 9.9 mmol, 0.5 equiv) was added dropwise, A white precipitate appeared immediately, which was filtered under reduced pressure to give 3.2 g of a colorless solid, 82%.

2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate Preparation Products And Raw materials

Raw materials

Preparation Products

2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate Suppliers

Global( 160)Suppliers

Supplier	Tel	Country	ProdList	Advantage	Inquiry
A.J Chemicals	91-9810153283	New Delhi, India	6124	58	Inquiry
Suzhou Victorypharm Co.,Ltd.	+86-13916956214	China	1301	58	Inquiry
Capot Chemical Co.,Ltd.	571-85586718 +8613336195806	China	29798	60	Inquiry
Hangzhou FandaChem Co.,Ltd.	008657128800458; +8615858145714	China	9338	55	Inquiry
ATK CHEMICAL COMPANY LIMITED	+undefined-21-51877795	China	32760	60	Inquiry
career henan chemical co	+86-0371-86658258 +8613203830695	China	29901	58	Inquiry
Zhejiang ZETian Fine Chemicals Co. LTD	+8618957127338	China	2141	58	Inquiry
Shanghai Worldyang Chemical Co.,Ltd.	,+86-21-56795779; +8613651600618	China	1080	58	Inquiry
Chongqing Chemdad Co., Ltd	+86-023-6139-8061 +86-86-13650506873	China	39916	58	Inquiry
Guangzhou Yuheng Pharmaceutical Technology Co., Ltd	+8613580539051	CHINA	21149	58	Inquiry

Supplier	Advantage
A.J Chemicals	58
Suzhou Victorypharm Co.,Ltd.	58
Capot Chemical Co.,Ltd.	60
Hangzhou FandaChem Co.,Ltd.	55
ATK CHEMICAL COMPANY LIMITED	60
career henan chemical co	58
Zhejiang ZETian Fine Chemicals Co. LTD	58
Shanghai Worldyang Chemical Co.,Ltd.	58
Chongqing Chemdad Co., Ltd	58
Guangzhou Yuheng Pharmaceutical Technology Co., Ltd	58

2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate Spectrum

2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate(1041026-71-4)¹HNMR 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate(1041026-71-4)FT-IR

1041026-71-4(2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxylate)Related Search:

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3-Azabicyclo[3.1.0]hexane-3,6-dicarboxylic acid 3-tert-butyl ester 7-Boc-1,7-diaza-spiro[4.4]nonane Tert-butyl 2,6-diazaspiro[3.4]octane-6-carboxylate 1-BENZYL-OCTAHYDRO-PYRROLO[3,4-B]PYRROLE 2-(3-(TERT-BUTOXYCARBONYL)-3-AZASPIRO[5.5]UNDECAN-9-YL)ACETIC ACID

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2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester heMioxylate 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid, 1,1-diMethylethyl ester, ethanedioate (2:1) 1-Boc-2,6-diazaspiro[3.3]heptane heMioxalate, 97% tert-Butyl 2,6-diazaspiro[3.3]heptane-2-carboxylate, hemioxalate salt 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid, 1,1-diMethylethyl ester, heMioxalate 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid 1,1-dimethylethyl ester ethanedioate tert-Butyl 2,6-diazaspiro[3,3]heptane-2-carboxylate hemioxalate 2,6-diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester oxalate 2,6-diaza-spiro[3.3]heptane-2-carboxylic acid tert-butyl ester, oxalic acid salt 2-Boc-2,6-diazaspiro[3.3]heptane Hemioxalate 2-Methyl-2-propanyl 2,6-diazaspiro[3.3]heptane-2-carboxylate ethanedioate 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester hemioxalate 2,6-Diazaspiro[3.3]heptane, N2-BOC protected hemioxalate 2,6-Diazaspiro[3.3]heptane-2-carboxylic acid ethanedioate, 1,1-dimethylethyl ester 2-Methyl-2-propanyl 2,6-diazaspiro[3.3]heptane-2-carboxylate ethanedioate (2:1) 1-Boc-2,6-diazaspiro[3.3]heptanehemioxalate,97% 2,6-diazo-heterospiro [3,3] heptane-2-carboxylic acid tert-butyl semicarbamate 6-diazaspiro[3.3]heptane-2-carboxylate oxalate tert-butyl 2,6-diazaspiro[3.3]heptane-2-carboxylate oxalate tert-Butyl 2,6-diazaspiro[3.3]heptane-2-carboxylate oxalate(2:1) 3-Oxazolidinecarboxylicacid,2,2-dimethyl-4-(2-oxoethyl)-,1,1-dimethylethylester,(10S)- 2-Boc-2,6-Diazaspiro[3.3]heptane ethanedioate (2:1) ert-Butyl 2,6-diazaspiro[3,3]heptane-2-carboxylate hemioxalate tert-Butyl 2,6-diazaspiro[3.3]heptane-2-carboxylate semioxalate 1041026-71-4 2C10H18N2O2C2H2O4