N,N'-Bis(phenyl)benzamidine
- CAS No.
- 2556-46-9
- Chemical Name:
- N,N'-Bis(phenyl)benzamidine
- Synonyms
- AURORA KA-4079;TIMTEC-BB SBB008627;N,N'-DIPHENYLBENZAMIDINE;N1,N2-Diphenylbenzamidine;N,N'-Bis(phenyl)benzamidine;N,N'-Diphenylbenzenecarboxamidine;Benzenecarboximidamide, N,N'-diphenyl-
- CBNumber:
- CB8404383
- Molecular Formula:
- C19H16N2
- Molecular Weight:
- 272.34
- MOL File:
- 2556-46-9.mol
- MSDS File:
- SDS
- Modify Date:
- 2023/1/11 10:46:38
N,N'-Bis(phenyl)benzamidine Chemical Properties,Uses,Production
Preparation
To a three-necked, round-bottomed flask equipped with a mechanical stirrer, dropping funnel, and condenser is added 90.0 gm (0.46 mole) of pure dry benzanilide (see Note a) and 95 gm (0.46 mole) of phosphorus pentachloride (see Note b). The mixture is stirred to reduce the lumps and then heated for ½ hr at 110°C and 1½hr at 160°C, or until the evolution of hydrogen chloride ceases. Then 36.4 gm (0.46 mole) of KOH-dried pyridine (see Note c) is added with stirring, followed by 42.4 gm (0.46 mole) of freshly distilled aniline. The reaction mixture is heated at 160°C for about 20 min to discharge the red color, cooled to about 90°C, and 250 ml of water is added dropwise to precipitate the product in granular form. The product is filtered and added to 500 ml of 28% aqueous ammonia. The mixture is stirred while gently warming for 1 hr, filtered, dried, and recrystallized from 80% ethanol (8-10 ml/gm product) to afford 73-80% product, m.p. 144-145°C.
N,N'-Bis(phenyl)benzamidine Preparation Products And Raw materials
Raw materials
Preparation Products
N,N'-Bis(phenyl)benzamidine Suppliers
Supplier | Tel | Country | ProdList | Advantage | Inquiry |
---|---|---|---|---|---|
ABCR GmbH & CO. KG | 49 721 95061 0 | Germany | 6846 | 75 | Inquiry |
Baoji Didu Pharmaceutical and Chemical Co., Ltd | 029-81148929 13186179623 | China | 10011 | 58 | Inquiry |
Apin Chemicals Ltd. | +44 1235 832515 | United Kingdom | 6811 | 42 | Inquiry |
VWR International | 800 932 5000 | United Kingdom | 6554 | 82 | Inquiry |
Alfa Aesar | 1 888 343-8025 Specialty/Bulk | United States | 6823 | 81 | Inquiry |
Frinton Laboratories, Inc. | 877-FRINTON (toll free) | United States | 1460 | 61 | Inquiry |
3B Scientific Corporation | 847 281 9822 | United States | 6971 | 56 | Inquiry |
Aurora Fine Chemicals Ltd. | [43] 316586738 | Austria | 6625 | 72 | Inquiry |
Service Chemical Inc. | 888-895-6920 | Germany | 6373 | 71 | Inquiry |
Eurolabs Limited | 44 1625 850089 | United Kingdom | 6323 | 46 | Inquiry |
Supplier | Advantage |
---|---|
ABCR GmbH & CO. KG | 75 |
Baoji Didu Pharmaceutical and Chemical Co., Ltd | 58 |
Apin Chemicals Ltd. | 42 |
VWR International | 82 |
Alfa Aesar | 81 |
Frinton Laboratories, Inc. | 61 |
3B Scientific Corporation | 56 |
Aurora Fine Chemicals Ltd. | 72 |
Service Chemical Inc. | 71 |
Eurolabs Limited | 46 |
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