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N,N'-Bis(phenyl)benzamidine

N,N'-Bis(phenyl)benzamidine Structure
CAS No.
2556-46-9
Chemical Name:
N,N'-Bis(phenyl)benzamidine
Synonyms
AURORA KA-4079;TIMTEC-BB SBB008627;N,N'-DIPHENYLBENZAMIDINE;N1,N2-Diphenylbenzamidine;N,N'-Bis(phenyl)benzamidine;N,N'-Diphenylbenzenecarboxamidine;Benzenecarboximidamide, N,N'-diphenyl-
CBNumber:
CB8404383
Molecular Formula:
C19H16N2
Molecular Weight:
272.34
MOL File:
2556-46-9.mol
MSDS File:
SDS
Modify Date:
2023/1/11 10:46:38

N,N'-Bis(phenyl)benzamidine Properties

Melting point 125-129 °C
Boiling point 441.6±18.0 °C(Predicted)
Density 1.03±0.1 g/cm3(Predicted)
pka 7.70±0.10(Predicted)

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS07
Signal word  Warning
Hazard statements  H302-H413
Precautionary statements  P273-P301+P312-P280
Hazard Codes  Xn
Risk Statements  22
WGK Germany  3
10
HS Code  2921599090

N,N'-Bis(phenyl)benzamidine Chemical Properties,Uses,Production

Preparation

To a three-necked, round-bottomed flask equipped with a mechanical stirrer, dropping funnel, and condenser is added 90.0 gm (0.46 mole) of pure dry benzanilide (see Note a) and 95 gm (0.46 mole) of phosphorus pentachloride (see Note b). The mixture is stirred to reduce the lumps and then heated for ½ hr at 110°C and 1½hr at 160°C, or until the evolution of hydrogen chloride ceases. Then 36.4 gm (0.46 mole) of KOH-dried pyridine (see Note c) is added with stirring, followed by 42.4 gm (0.46 mole) of freshly distilled aniline. The reaction mixture is heated at 160°C for about 20 min to discharge the red color, cooled to about 90°C, and 250 ml of water is added dropwise to precipitate the product in granular form. The product is filtered and added to 500 ml of 28% aqueous ammonia. The mixture is stirred while gently warming for 1 hr, filtered, dried, and recrystallized from 80% ethanol (8-10 ml/gm product) to afford 73-80% product, m.p. 144-145°C.
Preparation ofN,N'-Diphenylbenzamidine

N,N'-Bis(phenyl)benzamidine Preparation Products And Raw materials

Raw materials

Preparation Products

N,N'-Bis(phenyl)benzamidine Suppliers

Global( 20)Suppliers
Supplier Tel Country ProdList Advantage Inquiry
ABCR GmbH & CO. KG 49 721 95061 0 Germany 6846 75 Inquiry
Baoji Didu Pharmaceutical and Chemical Co., Ltd 029-81148929 13186179623 China 10011 58 Inquiry
Apin Chemicals Ltd. +44 1235 832515 United Kingdom 6811 42 Inquiry
VWR International 800 932 5000 United Kingdom 6554 82 Inquiry
Alfa Aesar 1 888 343-8025 Specialty/Bulk United States 6823 81 Inquiry
Frinton Laboratories, Inc. 877-FRINTON (toll free) United States 1460 61 Inquiry
3B Scientific Corporation 847 281 9822 United States 6971 56 Inquiry
Aurora Fine Chemicals Ltd. [43] 316586738 Austria 6625 72 Inquiry
Service Chemical Inc. 888-895-6920 Germany 6373 71 Inquiry
Eurolabs Limited 44 1625 850089 United Kingdom 6323 46 Inquiry
N,N'-DIPHENYLBENZAMIDINE TIMTEC-BB SBB008627 AURORA KA-4079 N,N'-Diphenylbenzenecarboxamidine N1,N2-Diphenylbenzamidine Benzenecarboximidamide, N,N'-diphenyl- N,N'-Bis(phenyl)benzamidine 2556-46-9 Building Blocks Organic Building Blocks Nitrogen Compounds Imines/Amidines Imines/Amidines Nitrogen Compounds Organic Building Blocks