3'-broMo-2'-메틸아세토페논

3'-broMo-2'-메틸아세토페논
3'-broMo-2'-메틸아세토페논 구조식 이미지
카스 번호:
52779-76-7
한글명:
3'-broMo-2'-메틸아세토페논
동의어(한글):
3'-broMo-2'-메틸아세토페논
상품명:
3'-bromo-2'-methylacetophenone
동의어(영문):
Fluralaner-006;Fluralaner Impurity 32;3'-broMo-2'-Methylacetophenone;3'-broMo-2'-Methylacetophenone;1-(3-Bromo-2-methylphenyl)ethanone;1-(3-bromo-2-methylphenyl)ethan-1-one;Ethanone, 1-(3-bromo-2-methylphenyl)-;1-(3-Bromo-2-Methylphenyl)Ethanone(WXC02293)
CBNumber:
CB02704889
분자식:
C9H9BrO
포뮬러 무게:
213.07
MOL 파일:
52779-76-7.mol

3'-broMo-2'-메틸아세토페논 속성

끓는 점
272.7±28.0 °C(Predicted)
밀도
1.388±0.06 g/cm3(Predicted)
저장 조건
Sealed in dry,Room Temperature
InChI
InChI=1S/C9H9BrO/c1-6-8(7(2)11)4-3-5-9(6)10/h3-5H,1-2H3
InChIKey
LBNWYNIGDUWAOQ-UHFFFAOYSA-N
SMILES
C(=O)(C1=CC=CC(Br)=C1C)C

안전

3'-broMo-2'-메틸아세토페논 C화학적 특성, 용도, 생산

Synthesis

To a stirred and refluxing Grignard-complex, previously prepared starting from 7.3 parts of magnesium, 52.6 parts of methyl iodide in 160 parts of ether, is added dropwise a solution of 19.6 parts of  3'-bromo-2'-methylbenzonitrile in 40 parts of ether. Upon completion, stirring at reflux is continued for 20 hours. The reaction mixture is cooled to 0 C and poured onto 500 parts of ice water while stirring vigorously. The ethereal phase is separated, dried and evaporated. The residue is boiled in 60 parts of a 6N hydrochloric acid solution for 10 minutes. The separated oil is extracted with ether. The extract is washed with water, dried and evaporated. The residue is distilled, yielding 3'-bromo-2'-methylacetophenone.

3'-broMo-2'-메틸아세토페논 준비 용품 및 원자재

원자재

준비 용품


3'-broMo-2'-메틸아세토페논 공급 업체

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