1-BROMO-2-BUTYNE
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1-BROMO-2-BUTYNE 속성
- 끓는 점
- 40-41 °C/20 mmHg (lit.)
- 밀도
- 1.519 g/mL at 25 °C (lit.)
- 굴절률
- n
20/D 1.508(lit.)
- 인화점
- 97 °F
- 저장 조건
- Inert atmosphere,Room Temperature
- 용해도
- 아세토니트릴과 혼합 가능.
- 물리적 상태
- 액체
- Specific Gravity
- 1.519
- 색상
- 투명하고 연한 황록색
- BRN
- 605306
- InChIKey
- LNNXOEHOXSYWLD-UHFFFAOYSA-N
- CAS 데이터베이스
- 3355-28-0(CAS DataBase Reference)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
| 위험 카페고리 넘버 | 10 | ||
|---|---|---|---|
| 안전지침서 | 16-24/25 | ||
| 유엔번호(UN No.) | UN 1993 3/PG 3 | ||
| WGK 독일 | 3 | ||
| F 고인화성물질 | 10-23 | ||
| 위험 등급 | 3 | ||
| 포장분류 | III | ||
| HS 번호 | 29033990 |
1-BROMO-2-BUTYNE C화학적 특성, 용도, 생산
화학적 성질
Clear pale yellow-greenish liquid용도
1-Bromo-2-butyne is used in the preparation of six to eight annulated ring compounds in reaction with indoles and pseudopterane (+/-)-Kallolide B, which is a marine natural product. Further, it acts as a precursor in the preparation of axially chiral teranyl compounds, alkylation of L-tryptophan methyl ester, 4-butynyloxybenzene sulfonyl chloride and mono-propargylated diene derivative. In addition to this, it is also used in the synthesis of isopropylbut-2-ynylamine, allenylcyclobutanol derivatives, allyl-[4-(but-2-ynyloxy)phenyl]sulfane, allenylindium and axially chiral teranyl compounds.제조 방법
1-bromo-2-butyne is obtained by reacting 2-butyn-1-ol and organic solvent, pyridine.First react bromoethane with metal magnesium in THF to prepare Grignard reagent, then add paraformaldehyde to Grignard reagent for Grignard reaction, separate and recover after Grignard reaction 2-butyn-1-ol, then mix 2-butyn-1-ol with organic solvent and pyridine, add phosphorus tribromide dropwise for bromination reaction, separate and recover the product after bromination reaction.일반 설명
1-Bromo-2-butyne is a propargyl bromide derivative. It is one of the constitutional isomer of bromo butyne. Its Br-loss threshold photoionization breakdown diagram has been analyzed to derive dissociative photoionization thresholds to C4H5+ production. It participates in the preparation of linagliptin.1-BROMO-2-BUTYNE 준비 용품 및 원자재
원자재
준비 용품
1-BROMO-2-BUTYNE 공급 업체
글로벌( 405)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| Shanghai Rochi Pharmaceutical Co.,Ltd. | 21-38751876 +8615000076078 |
info@rochipharma.com | China | 431 | 58 |
| Shaanxi Dideu Medichem Co. Ltd | +86-029-81138252 +86-18789408387 |
1057@dideu.com | China | 2873 | 58 |
| Hebei Mojin Biotechnology Co., Ltd | +86 13288715578 +8613288715578 |
sales@hbmojin.com | China | 12459 | 58 |
| Hebei Guanlang Biotechnology Co,.LTD | +86-19930503253; +8619930503252 |
daisy@crovellbio.com | China | 5838 | 58 |
| Hebei Dangtong Import and export Co LTD | 0086 15632927689 +8615632927689 |
admin@hbdangtong.com | China | 984 | 58 |
| Hebei Fengjia New Material Co., Ltd | +86-0311-87836622 +86-17333973358 |
sales06@hbduling.cn | China | 15695 | 58 |
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 |
info@fdachem.com | China | 20314 | 58 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 |
info@dakenam.com | China | 16216 | 58 |
| Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 |
info@tianfuchem.com | China | 21670 | 55 |
| Hangzhou FandaChem Co.,Ltd. | 008657128800458; +8615858145714 |
fandachem@gmail.com | China | 9337 | 55 |
1-BROMO-2-BUTYNE 관련 검색:
2-부틴
Levetiracetam
Lercanidipine
bamboo flavone
Adapalene
Rivaroxaban
1-Bromo-3-butyne,4-BROMO-1-BUTYNE
1-Bromo-1-butyne
1-BROMO-2-BUTYNE
1-BROMO-2-PENTYNE
1,4-DIBROMO-2-BUTYNE
1-(3-BROMO-1-PROPYNYL)NAPHTHALENE
1-BROMO-2-OCTYNE
2-Bromo-3-Butyne
2-Methyl-4-bromo-3-butyne-2-ol
3-Bromo-1-butyne
2-BROMO-3-HEXYNE
1-(3-BROMOPROP-1-YNYL)-3,5-DI(TRIFLUOROMETHYL)BENZENE