ChemicalBook >제품 카탈로그 >4-아이오도부틸아세테이트

4-아이오도부틸아세테이트

4-아이오도부틸아세테이트 구조식 이미지

카스 번호:: 40596-44-9

한글명:: 4-아이오도부틸아세테이트

동의어(한글):: 4-아이오도부틸아세테이트

상품명:: 4-IODOBUTYL ACETATE

동의어(영문):: 4-IODOBUTYL ACETATE;1-ACETOXY-4-IODOBUTANE;4-iodobutyl acetate 96%;4-ACETOXY-BUTAN-1-IODIDE;4-iodo-1-butanol acetate;1-Butanol, 4-iodo-, 1-acetate;4-Iodobutylacetate, 85%, tech.;4-Iodobutyl acetate, 97%, stab;ACETIC ACID 4-IODO-BUTYL ESTER;4-IODOBUTYL ACETATE, TECH., 85%

CBNumber:: CB1210301

분자식:: C6H11IO2

포뮬러 무게:: 242.05

MOL 파일:: 40596-44-9.mol

속성

안전

용도

공급 업체 57

4-아이오도부틸아세테이트 속성

끓는 점: 94-95 °C5.5 mm Hg(lit.)

밀도: 1.61 g/mL at 25 °C(lit.)

굴절률: n20/D 1.497(lit.)

인화점: 195 °F

용해도: 혼합하기가 어렵습니다.

물리적 상태: 액체

색상: Light green turbid

감도: Light Sensitive

CAS 데이터베이스: 40596-44-9(CAS DataBase Reference)

안전

위험 및 안전 성명
위험 및 사전주의 사항 (GHS)

위험품 표기	Xi
위험 카페고리 넘버	36/37/38
안전지침서	26-36/37/39
WGK 독일	3
HS 번호	29153900

그림문자(GHS):

신호 어:

Warning

유해·위험 문구:

암호	유해·위험 문구	위험 등급	범주	신호 어	그림 문자	P- 코드
H227	가연성 액체	인화성 액체	구분 4	경고		P210, P280, P370+P378, P403+P235,P501

예방조치문구:

P403+P235

환기가 잘 되는 곳에 보관하고 저온으로 유지하시오.

NFPA 704

	2
2		0

4-아이오도부틸아세테이트 C화학적 특성, 용도, 생산

화학적 성질

CLEAR DARK BROWN LIQUID

용도

4-Iodobutyl acetate is used in the preparation of tricyclohexyl(acetoxybutyl))phosphonium iodide, tri-n-hexyl(acetoxybutyl))phosphonium iodide

Synthesis Reference(s)

Synthetic Communications, 24, p. 951, 1994 DOI: 10.1080/00397919408020770

Synthesis

The synthesis of 4-IODOBUTYL ACETATE is as follows:Acetic acid (0.30mmol, 1.0 equivalent), CuI (0.03mmol, 10.0mol%, 5.7mg) and NaI (0.60mmol, 2.0 equivalent, 89.9mg) were added to a 10mL Schlenk tube equipped with a magnetic stirring device. Vacuum the flask with a pump and backfill it three times with nitrogen. Then, 1.0 mL tetrahydrofuran (12.30 mmol, 41.0 equivalence, 1 mL, c=0.30 M), deionized water (0.45 mmol, 1.5 equivalence) and TMSCF3 (0.36 mmol, 1.2 equivalence) were added under N2 atmosphere. The mixture is stirred at 150°C (thermostatic oil bath pot) for 12 hours. After cooling to room temperature, dilute the mixture with ethyl acetate (15 mL), wash with water and brine, and dry on anhydrousNa2SO4. After Extraction by EtOAc (5 mL x 3), the combined organic layer was dehydrated with anhydrousNa2SO4 and concentrated under reduced pressure. The crude product is purified by rapid chromatography on silica gel to obtain alkyl iodide.
synthesis of 4-IODOBUTYL ACETATE

4-아이오도부틸아세테이트 준비 용품 및 원자재

원자재

준비 용품

도덱-8-에닐아세테이트

4-아이오도부틸아세테이트 공급 업체

글로벌( 57)공급 업체

공급자	전화	이메일	국가	제품 수	이점
Hebei Mojin Biotechnology Co., Ltd	+86 13288715578 +8613288715578	sales@hbmojin.com	China	12460	58
Hefei TNJ Chemical Industry Co.,Ltd.	0551-65418671	sales@tnjchem.com	China	34571	58
Nanjing Triumpharm Co.,Ltd	+86-02586182925 +86-15105172550	info@triumpharm.com	China	129	58
SUZHOU SENFEIDA CHEMICAL CO.,LTD	+86-0512-83500002 +8615195660023	sales@senfeida.com	China	23053	58
Aladdin Scientific	+1-+1(833)-552-7181	sales@aladdinsci.com	United States	57511	58
Amadis Chemical Company Limited	571-89925085	sales@amadischem.com	China	131980	58
Mainchem Co., Ltd.	+86-0592-6210733	sale@mainchem.com	China	32360	55
Wuhan Aikang Chemical Co., Ltd.	13002132652	andriy@akkochemical.com	China	277	58
Meryer (Shanghai) Chemical Technology Co., Ltd.	021-61259108 18621169109	market03@meryer.com	China	40240	62
Alfa Aesar	400-6106006	saleschina@alfa-asia.com	China	30132	84

4-아이오도부틸아세테이트 관련 검색:

2-iodo-1-ethanol acetate 3-iodo-1-propanol acetate 5-iodo-1-pentanol acetate 6-Iodo-1-Hexanol 5-Chloropentanol 6-Chlorohexanol 3-Bromo-1-propanol 6-iodo-1-hexanol acetate 8-iodo-1-octanol acetate 9-iodo-1-nonanol acetate 7-iodo-1-heptanol acetate 10-iodo-1-nonanol acetate 2-(acetoxymethyl)-4-iodobutyl acetate 4-IODOBUTYL ACETATE 1,2,3-TRI-O-BENZOYL-4-DEOXY-ALPHA-L-FUCOPYRANOSE 4-IODOBUTYL BENZOATE 8-(IODOMETHYL)-1,8-DIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE 2,3,5-TRI(ACETYLOXY)-6-(IODOMETHYL)TETRAHYDRO-2H-PYRAN-4-YL ACETATE