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[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl-

[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl- 구조식 이미지

카스 번호:: 2086312-08-3

상품명:: [1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl-

동의어(영문):: 4-Tricyclo[3.3.1.13,7]Dec-1-yl-[1,1':3',1''-Terphenyl]-4'-Amine;4-tricyclo[3.3.1.13,7]dec-1-yl-[1,1':3',1''-Terphenyl]-4'-amine;1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl-;[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl-

CBNumber:: CB18800029

분자식:: C28H29N

포뮬러 무게:: 379.54

MOL 파일:: 2086312-08-3.mol

속성

안전

용도

공급 업체 18

[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl- 속성

끓는 점: 529.5±29.0 °C(Predicted)

밀도: 1.145±0.06 g/cm3(Predicted)

산도 계수 (pKa): 3.52±0.10(Predicted)

안전

[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl- C화학적 특성, 용도, 생산

용도

[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl-, also known as 4-(adamantane-1-yl)-[1,1':3',1“-terphenyl]-4’-amine, is an intermediate of photoelectric materials.

제조 방법

In a 3000L reactor, add 285kg of adamantyl phenyl triflate, 327.88kg of potassium carbonate, and 560L of water. Also, add 1000L of toluene, 304kg of boron ester, and 2.78kg of Pd (PPh ) Cl. Heat the mixture to 95°C and maintain reflux at this temperature. Monitor the progress of the reaction in the liquid phase. After completion, allow the mixture to separate into water and organic phases. Wash the organic phase twice with hot water. Add 5kg of activated carbon to the organic phase for decolorization. Filter the mixture and concentrate the toluene. To obtain a solid product, add ethanol and cool to 20°C. Perform suction filtration to obtain a powdery white solid. Repeat crystallization from toluene and ethanol three times to further purify the product [1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl-.

[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl- 준비 용품 및 원자재

원자재

준비 용품

[1,1':3',1''-Terphenyl]-4'-amine, 4-tricyclo[3.3.1.13,7]dec-1-yl- 공급 업체

글로벌( 18)공급 업체

공급자	전화	이메일	국가	제품 수	이점
Jiangsu Nata Opto-electronic Material Co.,Ltd.	+86-0512-62520998 +86-15030927757	gaoym@natachem.com	China	229	58
Shenzhen Nexconn Pharmatechs Ltd	+86-755-89396905 +86-15013857715	admin@nexconn.com	China	10312	58
Win-Win chemical CO., Limited	+86-0086-577-64498589 +86-15355981851	sales@win-winchemical.com	China	14351	58
ANHUI WITOP BIOTECH CO., LTD	+8615255079626	eric@witopchemical.com	China	23556	58
Shanghai Z&T Chemical Co., Ltd	+86-021-33561011 +8613818804961	Sales@ztchemical.com.cn	China	402	58
Zhengzhou Anbu Chem Co.,Ltd	+86-0371-88006763; +8615988602810	sales@anbuchem.com	China	3000	58
Shanghai Mingrunda New Materials Technology Co., Ltd	+86 13482725029 13482725029	sales@mrdchem.com	China	1012	58
Xi'an Kaixiang Photoelectric Technology Co., Ltd.	17792373796	201997953@qq.com	China	554	55
Zhengzhou Huiju Chemical Co., Ltd.	0371-55900031 18137872243	2853979815@qq.com	China	10007	55
Win-Win Chemical CO., Limited	0577-64498589 15325081899	sales@win-winchemical.com	China	1085	58