2,3,6,7,12,13-헥사브로모트립티센
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2,3,6,7,12,13-헥사브로모트립티센 속성
- 녹는점
- >350 °C(Solv: acetone (67-64-1))
- 끓는 점
- 552.6±50.0 °C(Predicted)
- 밀도
- 2.351±0.06 g/cm3(Predicted)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
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신호 어: | Warning | |||||||||||||||||||||||||||||||||||
유해·위험 문구: |
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예방조치문구: |
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2,3,6,7,12,13-헥사브로모트립티센 C화학적 특성, 용도, 생산
용도
2,3,6,7,14,15-Hexabromo-9,10-dihydro-9,10-[1,2]benzenoanthracene can be used as impurity standard and reference substance, mainly used in laboratory research and development process and chemical production process middle.Synthesis
Triptycene (1.06 g, 4.18 mmol) was dissolved in chloroform (80 mL) in a round-bottom flask. Iron filings (30 mg) were added, and the solution was stirred at 25 ??C. Bromine (1.35 mL, 26.3 mmol) was added, and the solution was refluxed for 1 h, during which time the initially reddish-brown solution turned reddish-orange. The flask was removed from heat, and chloroform and excess bromine were removed under vacuum. The resulting brown powder was dissolved in chloroform (100 mL) and flushed through a pad of silica using additional chloroform as eluent (100 mL). The filtrate was evaporated to dryness. The crude white powder (2.83 g, 98%) was crystallized from acetone yielding C20H8Br6 ?¤ (acetone)2 (0.88 g, 29%), mp >350 ??C. The mother liquor was evaporated and the residue was crystallized from acetone to afford a second crop of crystals (0.97 g, C20H8Br6 ?¤ (acetone)2, 32%). The combined yield was 1.85 g, 61%: 2-H yield 2.83 g, 98%
2,3,6,7,12,13-헥사브로모트립티센 준비 용품 및 원자재
원자재
준비 용품
2,3,6,7,12,13-헥사브로모트립티센 공급 업체
글로벌( 45)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
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Jilin Chinese Academy of Sciences - Yanshen Technology Co., Ltd. | 0431-80514535 13634302652 |
Extension@chemextension.com | CHINA | 967 | 58 |
Shaanxi Dideu Medichem Co. Ltd | +86-29-87569266 15319487004 |
1015@dideu.com | China | 4088 | 58 |
CHEMSOON CO.,LTD. | +8613761723174 |
sales01@chemsoon.com | China | 1211 | 58 |
Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 |
sale04@alfachem.cn | China | 13326 | 58 |
Shanghai Daeyeon Chemicals Co., Ltd | 021-64478606 +8615900664856 |
daeyeon001@vip.163.com | China | 2062 | 58 |
Career Henan Chemica Co | +86-0371-86658258 +8613203830695 |
laboratory@coreychem.com | China | 30250 | 58 |
Shanxi Xuanran Import and Export Trade Co., Ltd. | +8617735180244 |
mike_yan@xuanranglobal.com | CHINA | 4022 | 58 |
Alfa Chemistry | |
Info@alfa-chemistry.com | United States | 24072 | 58 |
Zhengzhou Anhuida Chemical Co., Ltd | +8615903659408 |
admin@ahdchem.com | China | 297 | 58 |
SUZHOU SENFEIDA CHEMICAL CO.,LTD | +86-0512-83500002 +8615195660023 |
sales@senfeida.com | China | 23048 | 58 |
2,3,6,7,12,13-헥사브로모트립티센 관련 검색:
9,10[1',2']-Benzenoanthracene-2,7,14-triamine, 9,10-dihydro-
9,10[1',2']-Benzenoanthracene-9,10-dicarboxylic acid
9,10[1',2']-Benzenoanthracene, 2,3,6,7,14,15-hexaethynyl-9,10-dihydro-
9,10-[1,2]benzenoanthracene-2,3,6,7,14,15(9H,10H)-hexaone
2,6,14-trioltriptycene
2,6,14-tribromotriptycene
2,3,6,7,14,15-Hexaaminotriptycene hexahydrochloride
2,6,14-triaminotriptycene
2,6,14-triiodotriptycene