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1,3-BIS(3-아미노펜옥시)벤젠

1,3-BIS(3-아미노펜옥시)벤젠 구조식 이미지

카스 번호:: 10526-07-5

한글명:: 1,3-BIS(3-아미노펜옥시)벤젠

동의어(한글):: 1,3-BIS(3-아미노펜옥시)벤젠

상품명:: 1,3-Bis(3-aminophenoxy)benzene

동의어(영문):: TPE-M;1,3,3-APB;RESORCINOL BIS(3-AMINOPHENYL) ETHER;APB-133;TIMTEC-BB SBB008356;1,3-BIS(3-AMINOPHENO;1,3-Bis(3-aminophenoxy;3,3'-Phenylenedioxydianiline;1,3-Bis(m-aminophenoxy)benzene;3,3-m-Phenylenebis(oxyaniline)

CBNumber:: CB8313496

분자식:: C18H16N2O2

포뮬러 무게:: 292.33

MOL 파일:: 10526-07-5.mol

속성

안전

용도

공급 업체 239

1,3-BIS(3-아미노펜옥시)벤젠 속성

녹는점: 108°C

끓는 점: 479.9±30.0 °C(Predicted)

밀도: 1.243

저장 조건: Keep in dark place,Inert atmosphere,Room temperature

수용성: 물에 불용성

물리적 상태: powder to crystal

산도 계수 (pKa): 4.29±0.10(Predicted)

색상: White to Light yellow to Light orange

InChI: InChI=1S/C18H16N2O2/c19-13-4-1-6-15(10-13)21-17-8-3-9-18(12-17)22-16-7-2-5-14(20)11-16/h1-12H,19-20H2

InChIKey: DKKYOQYISDAQER-UHFFFAOYSA-N

SMILES: C1(OC2C=CC=C(N)C=2)=CC=CC(OC2C=CC=C(N)C=2)=C1

CAS 데이터베이스: 10526-07-5(CAS DataBase Reference)

EPA: Benzenamine, 3,3'-[1,3-phenylenebis(oxy)]bis- (10526-07-5)

안전

위험 및 안전 성명

위험 카페고리 넘버	20/21/22
안전지침서	26-36/37/39
HS 번호	29222990
기존화학 물질	2009-3-3948

그림문자(GHS):

신호 어:

Warning

유해·위험 문구:

암호	유해·위험 문구	위험 등급	범주	신호 어	그림 문자	P- 코드

예방조치문구:

P261	분진·흄·가스·미스트·증기·...·스프레이의 흡입을 피하시오.
P264	취급 후에는 손을 철저히 씻으시오.
P264	취급 후에는 손을 철저히 씻으시오.
P270	이 제품을 사용할 때에는 먹거나, 마시거나 흡연하지 마시오.
P271	옥외 또는 환기가 잘 되는 곳에서만 취급하시오.
P280	보호장갑/보호의/보안경/안면보호구를 착용하시오.
P501	...에 내용물 / 용기를 폐기 하시오.

NFPA 704

	1
1		0

1,3-BIS(3-아미노펜옥시)벤젠 C화학적 특성, 용도, 생산

화학적 성질

1,3-Bis(3-aminophenoxy)benzene, also known as TIMTEC-BB SBB008356, is a Light yellow to yellow solid. It has slight solubility in methanol but is insoluble in water. To maintain its stability, it is recommended to store it in a cool and dark place. However, it is incompatible with oxidizing agents and should not be stored or handled near them to avoid any hazardous reactions.

용도

1,3-Bis(3-aminophenoxy)benzene is an intermediate compound used in the production of synthetic materials, such as PI (polyimide) films and polyimide materials.

제조 방법

1,3-Bis(3-aminophenoxy)benzene is a reactive monomer commonly utilized in the synthesis of polyurethane coatings. This compound is processed at 200 degrees Celsius and has a viscosity of 1.5-2.0 centipoise at 25 degrees Celsius. Its chemical structure consists of three amine groups that are ether linked to a benzene ring with one hydroxyl group on the phenoxy side chain. The monomer can be synthesized via acylation reaction or polymerization process, typically through heating with a catalyst. The resulting product is thermally stable and resistant to heat up to 250 degrees Celsius.

Synthesis

In the 500mL four neck flasks that have agitator, reflux exchanger and dean stark trap, add the 3-amino phenol of 71.5g (0.655mol), 49 quality % aqueous sodium hydroxide solutions, 250gDMI and the 50g toluene of 53.5g (0.655mol).Flask contents is heated to 180 ℃ and stir and to feed nitrogen simultaneously, and azeotropic is removed toluene and water.Subsequently, the flask inclusion is cooled to room temperature and transfers in the 600mL autoclave that has agitator.
Subsequently, add 1 of 34g (0.298mol), 3-two fluorobenzene; Seal this reactor; To wherein being blown into nitrogen; After this, autoclave is heated to 200 ℃; And order is reflected to be carried out under 200 ℃ 53 hours.After this, cool off this autoclave, by the reaction mixture of high efficiency liquid chromatography (after this abbreviating HPLC as) analysis part.The result is 1,3-Bis(3-aminophenoxy)benzene is 82% (with respect to 1,3-two fluorobenzene).

1,3-BIS(3-아미노펜옥시)벤젠 준비 용품 및 원자재

원자재

1,3-비스(3-니트로페녹시)벤젠 디브로모벤젠(1,3-) 3-아미노페놀

준비 용품

1,3-BIS(3-아미노펜옥시)벤젠 공급 업체

글로벌( 239)공급 업체

공급자	전화	이메일	국가	제품 수	이점
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	16216	58
Shanghai Daeyeon Chemicals Co., Ltd	021-64478606 +8615900664856	daeyeon001@vip.163.com	China	2062	58
CHINATECH(TIANJIN) CHEMICAL CO.,LTD.	+86-18222270857 +86-18222265956	sales5@chinatechem.com	China	64	58
Henan Allgreen Chemical Co.,LTD	+86-37155567971 +86-13633837469	info@allgreenchem.com	China	5986	58
LEAP CHEM CO., LTD.	+86-852-30606658	market18@leapchem.com	China	24738	58
Henan Fengda Chemical Co., Ltd	+86-371-86557731 +86-13613820652	info@fdachem.com	China	20314	58
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21670	55
Hangzhou FandaChem Co.,Ltd.	008657128800458; +8615858145714	fandachem@gmail.com	China	9337	55
career henan chemical co	+86-0371-86658258 +8613203830695	sales@coreychem.com	China	29897	58
Accela ChemBio Inc.	(+1)-858-699-3322	info@accelachem.com	United States	19965	58

1,3-BIS(3-아미노펜옥시)벤젠 관련 검색:

4,4'-(1,3-페닐렌다이옥시)다이아닐린 3-아미노페놀 3,3',4,4'-벤조페논 테트라카본산 2무수물 4,4'-[[2,2,2-트리플루오로-1-(트리플루오로메틸)에틸리덴]비스(4,1-페 닐렌옥시)]비스벤젠아민 4,4'-Bis(4-aminophenoxy)biphenyl 4,4'-DIAMINOBIPHENYL-2,2'-DICARBOXYLIC ACID 1,4-BIS(4-AMINOPHENOXY)BENZENE(144BAPB),1,4-Bis(p-aminophenoxy)benzene,1,4-BIS(4-AMINOPHENOXY)BENZENE 1,4-BIS(3-AMINOPHENOXY)BENZENE 1,3-DIPHENOXYBENZENE 1,3-Bis(3-aminophenoxy)benzene 3-PHENOXYPHENOL 3-PHENOXYANILINE 3-(3-METHOXY-PHENOXY)-PHENYLAMINE 1,2-BIS(4-AMINOPHENOXY)BENZENE(124BAPB) 3,3'-(1,3-PHENYLENEDIOXY)DIANILINE-15N2 1,2-BIS(3-AMINOPHENOXY)BENZENE