뷰틸 아세트알
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뷰틸 아세트알 속성
- 끓는 점
- 143°C/760mmHg
- 밀도
- 0.829 g/mL at 20 °C
- 굴절률
- n20/D1.396
- 인화점
- 30 °C
- 저장 조건
- Flammables area
- 물리적 상태
- 액체
- 색상
- 무색의
- BRN
- 1697910
- LogP
- 2.041 (est)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
| 위험품 표기 | Xi | ||
|---|---|---|---|
| 위험 카페고리 넘버 | 10-36/38 | ||
| 안전지침서 | 26-37/39-16 | ||
| 유엔번호(UN No.) | UN 1993C 3 / PGIII | ||
| WGK 독일 | 3 | ||
| HS 번호 | 29329990 | ||
| 기존화학 물질 | KE-10337 |
뷰틸 아세트알 C화학적 특성, 용도, 생산
화학적 성질
Clear colorless liquid제조 방법
To a three-necked flask equipped with an air-tight mechanical stirrer, dropping funnel, reflux condenser, and drying tube, are added 3.0 gm (1.25 gm-atom) magnesium turnings, 50 ml of dry ether, and a small crystal of iodine. Then 5 gm of rt-butyl bromide is added dropwise until 171.0 gm (1.25 mole) has been added. The reaction takes about ½ - l h r if the reaction mixture is cooled. The solution is refluxed for ½ hr, cooled to 50°C, and then 148 gm (1.0 mole) of triethyl orthoformate is added dropwise over a ½-hr period. The reaction mixture is refluxed for 16 hr, crushed ice added to decompose the excess Grignard reagent, the ether separated and washed with water. The water layer is added to a separatory funnel containing 200 ml of ether, treated with acetic acid to pH 7.0, shaken, and the ether separated. The latter ether layer is washed with 10% aqueous sodium carbonate, water, and dried. The latter water layer is extracted twice again with ether (200 ml). The combined ether layers are dried over potassium carbonate and fractionated to afford 128 gm (80%), b.p. 143°-144°.
뷰틸 아세트알 준비 용품 및 원자재
원자재
4,4-다이메톡시-1-부텐
1-부테닐에틸에테르
Triethyl orthobutyrate
헥센-1-일-알데히드
디에틸설페이트
n-부탄올
에틸알코올
오소포름산에틸
크로톤알데하이드
트리에톡시실란
N-프로피마그네슘브로마이드
준비 용품
뷰틸 아세트알 공급 업체
글로벌( 50)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| Shaanxi Dideu Medichem Co. Ltd | +86-029-81138252 +86-18789408387 |
1057@dideu.com | China | 3958 | 58 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 |
ivan@atkchemical.com | China | 32957 | 60 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 |
sales@tnjchem.com | China | 34563 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | 571-88938639 +8617705817739 |
info@dycnchem.com | China | 52849 | 58 |
| GIHI CHEMICALS CO.,LIMITED | +8618058761490 |
info@gihichemicals.com | China | 49978 | 58 |
| Aladdin Scientific | +1-+1(833)-552-7181 |
sales@aladdinsci.com | United States | 52924 | 58 |
| Amadis Chemical Company Limited | 571-89925085 |
sales@amadischem.com | China | 131957 | 58 |
| Mainchem Co., Ltd. | -- |
sarah@mainchem.com | China | 6567 | 58 |
| J & K SCIENTIFIC LTD. | 010-82848833 400-666-7788 |
jkinfo@jkchemical.com | China | 96815 | 76 |
| Meryer (Shanghai) Chemical Technology Co., Ltd. | 021-61259108 18621169109 |
market03@meryer.com | China | 40228 | 62 |