Standard

In the analysis work, it often demanded to apply high-quality compound with the exact content being accurate in order to be compared as the detection control or used to calibrate the instrument, the compound is known as standard sample.
Standard refers to the standard substance used for measuring the potency of biological products. When the production department submits to a higher authority for approval of the quality standard of the biological product, they should also provide the standard sample (indicated in unit (μ)) used for measuring the potency of the tested product.

According to different application, the verification products can be divided into biological standard for the testing of biological products, endocrine drugs, antibiotics and other bioassay and chemical standards including:
1 chemical standards used for calibration of the instrument;
2 chemical reference standards used for calibration of the ultraviolet or infrared spectrum of the drugs;
3 control standards used for the purity test of drugs as well as the impurity control or as the control standards for content determination of the medicine.

In the page 67 of the appendix in the People's Republic of China Pharmacopoeia 1990 1st edition, we can find hundreds kinds of standards including bornyl ester acetate, eugenol and panaxadiol as well as 39 kinds of control medicine for the purify inspection of traditional Chinese medicine, impurity control or the content determination.

International standards
This refers to standard sample, with the potency units of the existing international standard sample potency units as baseline, undergoing further calibration of its potency units on the basis of a wide range of international cooperation. Its potency is expressed in 1U. For a certain product, for the establishment of the first international standard sample, the determination of its potency units should be consulted and decided by the Committee of Experts before the announcement. The international standard is a standard reference substance for worldwide preparation of national standards, so that the international standards can achieve unity.

Reagents and standards
All reagents in the food analysis laboratories should be clearly labeled to indicate the following: 1 name; 2 the date of preparation; 3 Signature from the people in charge; 4 if necessary, we need to add content such as safety and validity and so on.
Most food analysis should use standard sample as reference for qualitative and quantitative determination. The standard sample should be classified according to the following classification methods: 1 international standard; 2 national standards; 3 internal standard; 4 other standards.
Receptacle for reference standards should be clearly affixed to the label, to indicate the following: 1 name; 2 standard document number; 3 Opening times; 4 Validity; 5 Signature.
In addition, the laboratory should keep all the necessary specific files for all the necessary reference standards.
Capacity analysis standard solution should also be strictly managed. It should be clearly posted on all the standard solution containers with labels to indicate: 1 name; 2 concentration; 3 formulation date; 4 No of formulated procedures; 5 storage conditions; 6 validity; 7 Signature from people in charge.

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Structure Chemical Name CAS MF
Nicorandil Impurity 6 Nicorandil Impurity 6
VIOLURIC ACID VIOLURIC ACID 87-39-8 C4H3N3O4
Cefaclor Impurity 2 Cefaclor Impurity 2 722547-49-1 C17H18N2O3
Cefodizime Impurity F Cefodizime Impurity F
Olaparib Impurity F Olaparib Impurity F
Ornidazole Impurity G Ornidazole Impurity G
Pidotimod Impurity L Pidotimod Impurity L
Tadalafil Impuirty 20 Tadalafil Impuirty 20 2924098-58-6
Tenofovir Impurity 53 Tenofovir Impurity 53
(S)-3-(4-benzylphenoxy)tetrahydrofuran (S)-3-(4-benzylphenoxy)tetrahydrofuran C17H18O2
Ampicillin Ampicillin 1207726-28-0 C24H26N4O5S
ethyl 2-(4-(sec-butoxy)-3-cyanophenyl)-4-methylthiazole-5-
carboxylate ethyl 2-(4-(sec-butoxy)-3-cyanophenyl)-4-methylthiazole-5- carboxylate 2375033-35-3 C18H20N2O3S
(S)-Indacaterol (S)-Indacaterol 1384188-70-8 C24H29ClN2O3
Aripiprazole Impurity 47 Aripiprazole Impurity 47 2250242-47-6 C27H33Cl2N3O3
Aripiprazole Impurity 47 Aripiprazole Impurity 47 2250242-47-6 C27H33Cl2N3O3
Cefminox Sodium  Impurity 3 Cefminox Sodium Impurity 3 1420072-83-8 C16H21N7O6S4
Edaravone Impurity 26 Edaravone Impurity 26 152494-76-3
Levofloxacin Impurity 24 Levofloxacin Impurity 24 C18H20FN3O4
Parecoxib N-Oxide Parecoxib N-Oxide
Rosuvastatin Impurity 84 Rosuvastatin Impurity 84
Timolol EP Impurity I Timolol EP Impurity I
172967-64-5 172967-64-5 172967-64-5 C18H16ClNO3
Pregabalin Impurity PD0224377 Pregabalin Impurity PD0224377 501665-97-0 C14H25NO6
Atracurium Impurity R Atracurium Impurity R
Fludarabine EP impurity K Fludarabine EP impurity K
Ropivacaine Impurity 28 Ropivacaine Impurity 28
Ropivacaine Impurity 6 Ropivacaine Impurity 6
Solifenacin ring opening Impurity 11 Solifenacin ring opening Impurity 11
Sugammadex sodium Org210839-1 Impurity Sugammadex sodium Org210839-1 Impurity
Sugammadex sodium Org284426-1 Impurity Sugammadex sodium Org284426-1 Impurity
Bendamustine Related Impurity 6 Bendamustine Related Impurity 6
Butyphthalide impurity 39 Butyphthalide impurity 39 1841089-57-3 C24H28O4
Butyphthalide impurity 45 Butyphthalide impurity 45
Dapoxetine impurity 18 Dapoxetine impurity 18
Febuxostat Impurity 76 Febuxostat Impurity 76
Febuxostat Impurity 91 Febuxostat Impurity 91
Ipratropium Bromide Impurity 1 Ipratropium Bromide Impurity 1 C20H29Br2NO3
Lenvatinib Impurity 18 Lenvatinib Impurity 18
Moxifloxacin Impurity 44 Moxifloxacin Impurity 44 1048972-52-6 C14H12FNO5
Nintedanib Impurity 32 Nintedanib Impurity 32
Olsalazine Impurity C Olsalazine Impurity C
Parecoxib sodium Impurity 33 Parecoxib sodium Impurity 33
Tofacitinib Impurity 96 Tofacitinib Impurity 96
Vildagliptin Impurity ZA5 Vildagliptin Impurity ZA5
Linagliptin Impurity CD10925 Linagliptin Impurity CD10925
Nintedanib Impurity N Nintedanib Impurity N
(2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chloro-3-(4- hydroxybenzyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chloro-3-(4- hydroxybenzyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate 1079083-63-8 C27H29ClO10
Vildagliptin Impurity 25 Vildagliptin Impurity 25 1563006-28-9 C7H10N2O2
(2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chloro-3- (4-methoxybenzyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chloro-3- (4-methoxybenzyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate 872980-38-6 C28H31ClO10
Vinorelbine Impurity DX Vinorelbine Impurity DX 89368-94-5 C46H55BrN4O8
1-hydroxypropan-2-yl 2-(2-(4-((4-chlorophenyl)(phenyl)
methyl)piperazin-1-yl)ethoxy)acetate compound with 2-
hydroxypropyl 2-(2-(4-((4-chlorophenyl)(phenyl)methyl)
piperazin-1-yl)ethoxy)acetate (1:1) hydrochloride 1-hydroxypropan-2-yl 2-(2-(4-((4-chlorophenyl)(phenyl) methyl)piperazin-1-yl)ethoxy)acetate compound with 2- hydroxypropyl 2-(2-(4-((4-chlorophenyl)(phenyl)methyl) piperazin-1-yl)ethoxy)acetate (1:1) hydrochloride
N-(2-(7-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)ethyl)acetamide N-(2-(7-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)ethyl)acetamide 178677-49-1 C15H21NO2
Eltrombopag Impurity 2 Eltrombopag Impurity 2
Dapoxetine Impurity 17 Dapoxetine Impurity 17
Avibactam Impurity Avibactam Impurity 2064219-26-5 C7H12N3NaO6S
(1s,4s)-4-((2-aminobenzyl)amino)cyclohexan-1-ol hydrochloride (1s,4s)-4-((2-aminobenzyl)amino)cyclohexan-1-ol hydrochloride C13H21ClN2O
Solifenacin impurity 23 Solifenacin impurity 23
Edaravone impurity DEE Edaravone impurity DEE
Linagliptin Impurity 49 Linagliptin Impurity 49
(1r,4r)-4-(7,9-dibromo-2,3-dihydro-1H-benzo[e][1,4]diazepin-4(5H)-yl)cyclohexanol hydrochloride (1r,4r)-4-(7,9-dibromo-2,3-dihydro-1H-benzo[e][1,4]diazepin-4(5H)-yl)cyclohexanol hydrochloride 2376577-10-3 C15H21Br2ClN2O
Procatero Impurity Procatero Impurity 90098-93-4 C11H9NO3
4-((2-amino-3,5-dibromobenzyl)amino)cyclohexanone hydrochloride 4-((2-amino-3,5-dibromobenzyl)amino)cyclohexanone hydrochloride C13H17Br2ClN2O
Pazufloxacin Impurity 5 Pazufloxacin Impurity 5 777824-29-0 C15H15FN2O2
Vonoprazan Impurity Z-4 Vonoprazan Impurity Z-4
Olanzapine impurity O Olanzapine impurity O C17H20N4S
Cabozantinib impurity 26 Cabozantinib impurity 26 2840522-80-5 C28H25ClFN3O5
Afatinib impurity 45 Afatinib impurity 45 99281-87-5 C5H9NO2
Afatinib impurity 45 Afatinib impurity 45 99281-87-5 C5H9NO2
Dapoxetine impurity 24 Dapoxetine impurity 24 1445281-20-8 C20H20O4S
Tazobactam Impurity E Tazobactam Impurity E
Vildagliptin Impurity 42 Vildagliptin Impurity 42
Canagliflozin Impurity 45 Canagliflozin Impurity 45
Pralatrexate Impurity 5 Pralatrexate Impurity 5
Pitavastatin Impurity 61 Pitavastatin Impurity 61
Sitafloxacin Impurity 17 Sitafloxacin Impurity 17
Cilastatin Isomer Impurity Cilastatin Isomer Impurity
Prednicarbate Impurity E Prednicarbate Impurity E
Olprinone Impurity B Olprinone Impurity B
Atracurium Impurity 28 Atracurium Impurity 28
Canagliflozin Impurity 51 Canagliflozin Impurity 51
Canagliflozin Impurity 67 Canagliflozin Impurity 67
Cefazolin Impurity Q Cefazolin Impurity Q
Acyclovir Impurity 13 Acyclovir Impurity 13
Afatinib impurity 48 Afatinib impurity 48
Afatinib impurity 48 Afatinib impurity 48
Cabozantinib impurity M Cabozantinib impurity M
Rotigotine Impurity 8 Rotigotine Impurity 8
Palbociclib-025 Palbociclib-025 2174002-16-3 C25H29N7O3
IRBESARTAN RELATED COMPOUND A (25 MG) (1-PENTANOYLAMINO-CYCLOPENTANECARBOXYLIC ACID [2'-(1H-TETRAZOL-5-YL)-BIPHENYL-4-YLMETHYL]-AMIDE) IRBESARTAN RELATED COMPOUND A (25 MG) (1-PENTANOYLAMINO-CYCLOPENTANECARBOXYLIC ACID [2'-(1H-TETRAZOL-5-YL)-BIPHENYL-4-YLMETHYL]-AMIDE) 748812-53-5 C25H30N6O2
FENOFIBRATE RELATED COMPOUND C (25 MG) (1-METHYLETHYL 2-[[2-[4-(4-CHLOROBENZOYL)PHENOXY]-2-METHYLPROPANOYL]OXY]-2-METHYLPROPANOATE) FENOFIBRATE RELATED COMPOUND C (25 MG) (1-METHYLETHYL 2-[[2-[4-(4-CHLOROBENZOYL)PHENOXY]-2-METHYLPROPANOYL]OXY]-2-METHYLPROPANOATE) 217636-48-1 C24H27ClO6
(S-(R* S*))-(+)-N-(1-PHENYLETHYL)-1- AZ& (S-(R* S*))-(+)-N-(1-PHENYLETHYL)-1- AZ& 120570-09-4 C15H24Cl2N2
CLOPIDOGREL  RELATED  COMPOUND  B (20 MG) (METHYL(+/-)-(O-CHLOROPHENYL)-4,5-DIHYDROTHIE-NO[2,3-C]PYRIDINE-6(7H)-ACETATE, HYDROCHLORIDE) CLOPIDOGREL RELATED COMPOUND B (20 MG) (METHYL(+/-)-(O-CHLOROPHENYL)-4,5-DIHYDROTHIE-NO[2,3-C]PYRIDINE-6(7H)-ACETATE, HYDROCHLORIDE) 144750-52-7 C16H16ClNO2S.ClH
VERAPAMIL RELATED COMPOUND B (50 MG) (AL-PHA-[2-[[2-(3,4-DIMETHOXYPHENYL)-ETHYL]METHYLA-MINO]ETHYL]-3,4-DIMETHOXY-ALPHA-(1-METHY-LETHYL)-BENZENEACETONITRILE MONOHYDROCHLORIDE) VERAPAMIL RELATED COMPOUND B (50 MG) (AL-PHA-[2-[[2-(3,4-DIMETHOXYPHENYL)-ETHYL]METHYLA-MINO]ETHYL]-3,4-DIMETHOXY-ALPHA-(1-METHY-LETHYL)-BENZENEACETONITRILE MONOHYDROCHLORIDE) 1794-55-4 C26H37ClN2O4
Cinacalcet Impurity 38 HCl Cinacalcet Impurity 38 HCl 938177-81-2 C21H24ClN
Norepinephrine Impurity 23 Norepinephrine Impurity 23 1528622-09-4 C9H13NO3
Brexpiprazole Impurity 77 Brexpiprazole Impurity 77 1783311-11-4 C12H14N2S
(S)-1-(isopropylamino)-3-(4-(2-methoxyethyl)phenoxy)propan-2-ol (S)-1-(isopropylamino)-3-(4-(2-methoxyethyl)phenoxy)propan-2-ol 114218-35-8 C15H26ClNO3
Recombinant Endo Beta-N-Acetylglucosaminidase (ENGASE) Recombinant Endo Beta-N-Acetylglucosaminidase (ENGASE)
1-Pentanone, 1-(2-hydroxy-5-methylphenyl)- 1-Pentanone, 1-(2-hydroxy-5-methylphenyl)- 150033-77-5 C12H16O2
3-methyl-2-pentylphenol 3-methyl-2-pentylphenol 1823068-39-8 C12H18O
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