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| | delphinine Basic information |
| Product Name: | delphinine | | Synonyms: | delphinine;(16S)-1α,6α,16-Trimethoxy-4-(methoxymethyl)-20-methylaconitane-8,13,14α-triol 8-acetate 14-benzoate;Aconitane-8,13,14-triol, 1,6,16-trimethoxy-4-(methoxymethyl)-20-methyl-, 8-acetate 14-benzoate, (1α,6α,14α,16β)-;Aconitane-8,13,14-triol,1,6,16-trimethoxy-4-(methoxymethyl)-20-methyl-, 8-acetate 14-benzoate, (1a,6a,14a,16b)- | | CAS: | 561-07-9 | | MF: | C33H45NO9 | | MW: | 599.72 | | EINECS: | 209-214-0 | | Product Categories: | | | Mol File: | 561-07-9.mol |  |
| | delphinine Chemical Properties |
| Melting point | 197.5-199° | | alpha | D20 +25° (ethanol) | | Boiling point | 650.15°C (rough estimate) | | density | 1.1925 (rough estimate) | | refractive index | 1.5960 (estimate) | | pka | 12.86±0.70(Predicted) | | Water Solubility | 20mg/L(25 ºC) |
| | delphinine Usage And Synthesis |
| Purification Methods | It crystallises from EtOH with 198-200o uncorrected (187.5-188.5o) and from Et2O or Me2CO. Its solubility at ~25o in EtOH, CHCl3 and Et2O is 4%, 5% and 10% respectively. In c 1, EtOH, it has [] 20 +22o changing to +19o in 4 hours. [Markwood J Am Chem Soc 16 931 1927.] The hydrochloride has m 214o(dec) from MeOH or MeOH/Et2O. [Weissner et al. Can J Chem 50 1925 1972, Jacobs & Craig J Biol Chem 127 363 1939, Beilstein 21 III/IV 2867.] |
| | delphinine Preparation Products And Raw materials |
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