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9-Benzyl-3,6-dibroMocarbazole

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Products Intro: Product Name:9-Benzyl-3,6-dibromocarbazole
CAS:118599-27-2
Purity:98
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Products Intro: Product Name:9-Benzyl-3,6-dibromocarbazole
CAS:118599-27-2
Purity:98% Min. Package:100g;1kg;5kg,10kg,25kg,50kg
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Products Intro: Product Name:9-Benzyl-3,6-dibroMocarbazole
CAS:118599-27-2
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Products Intro: Product Name:9-Benzyl-3,6-dibromo-9H-carbazole
CAS:118599-27-2
Purity:99%min Package:100g/bottle;500g/bottle;1kg/bottle;10kg/drum;50kg/drum;100kg/drum;1963T/drum;
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Products Intro: Product Name:9-Benzyl-3,6-dibroMocarbazole
CAS:118599-27-2
Purity:98% Package:1KG;USD|10KG;USD|25KG;USD

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9-Benzyl-3,6-dibroMocarbazole Basic information
Product Name:9-Benzyl-3,6-dibroMocarbazole
Synonyms:9-Benzyl-3,6-dibroMocarbazole;9-Benzyl-3,6-dibromocarbazole >;9H-Carbazole, 3,6-dibromo-9-(phenylmethyl)-;3,6-Dibromo-9-(phenylmethyl)-9H-carbazole
CAS:118599-27-2
MF:C19H13Br2N
MW:415.12
EINECS:
Product Categories:
Mol File:118599-27-2.mol
9-Benzyl-3,6-dibroMocarbazole Structure
9-Benzyl-3,6-dibroMocarbazole Chemical Properties
Melting point 160.0 to 164.0 °C
Boiling point 541.9±50.0 °C(Predicted)
density 1.59±0.1 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
form powder to crystal
color White to Light yellow
λmax357nm(CH3CN)(lit.)
InChIInChI=1S/C19H13Br2N/c20-14-6-8-18-16(10-14)17-11-15(21)7-9-19(17)22(18)12-13-4-2-1-3-5-13/h1-11H,12H2
InChIKeyQVFWRFBJSIUPAD-UHFFFAOYSA-N
SMILESN1(CC2=CC=CC=C2)C2=C(C=C(Br)C=C2)C2=C1C=CC(Br)=C2
CAS DataBase Reference118599-27-2
Safety Information
HS Code 2933.99.8290
MSDS Information
9-Benzyl-3,6-dibroMocarbazole Usage And Synthesis
SynthesisA solution of 13.33 g (0.0831 mol) Br2 in 20 mL glacial acetica cid was generally added by dropping funnel to another solution of 10.0 g (0.0389 mol) N-benzyl-9H-carbazole in 60 mL glacial acetic acid. The mixture was stirred for 24 h at room temperature. The mixture solution was poured into 500 mL water, and the resulting solid was filtered. The crude products were purified by washing (100 mL petroleum ether) and recrystallizing (ethyl acetate: petroleum ether = 1:4) to yield product 9-Benzyl-3,6-dibroMocarbazole as white needles (12.2 g, yield74.1percent).
9-Benzyl-3,6-dibroMocarbazole Preparation Products And Raw materials
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