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Methyl trans-3-(boc-amino)cyclobutanecarboxylate

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Products Intro: Product Name:methyl trans-3-(boc-amino)cyclobutanecarboxylate
CAS:1101173-77-6
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Products Intro: Product Name:methyl trans-3-(boc-amino)cyclobutanecarboxylate
CAS:1101173-77-6
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CAS:1101173-77-6
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Products Intro: Product Name:METHYL TRANS-3-(BOC-AMINO)CYCLOBUTANECARBOXYLATE
CAS:1101173-77-6
Purity:97% HPLC Package:1g;10g;100g;1kg
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Methyl trans-3-(boc-amino)cyclobutanecarboxylate Basic information
Product Name:Methyl trans-3-(boc-amino)cyclobutanecarboxylate
Synonyms:Methyl trans-3-(Boc-aMino)cyclobutanecarboxylate;trans-Methyl 3-((tert-butoxycarbonyl)amino)cyclobutanecarboxylate;Methyl trans-3-(Boc-amino)cyclobutanecarboxylate - SB7936;methyl 3-[(2-methylpropan-2-yl)oxycarbonylamino]cyclobutane-1-carboxylate;Cyclobutanecarboxylic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, trans-;methyl trans-3-(tert-butoxycarbonylamino)cyclobutanecarboxylate;Methyl trans-3-(Boc-aMino...
CAS:1101173-77-6
MF:C11H19NO4
MW:229.27
EINECS:
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Mol File:1101173-77-6.mol
Methyl trans-3-(boc-amino)cyclobutanecarboxylate Structure
Methyl trans-3-(boc-amino)cyclobutanecarboxylate Chemical Properties
Boiling point 314.1±31.0 °C(Predicted)
density 1.10±0.1 g/cm3(Predicted)
storage temp. 2-8°C
pka12.05±0.40(Predicted)
form solid
color White
Safety Information
HS Code 2922498590
MSDS Information
Methyl trans-3-(boc-amino)cyclobutanecarboxylate Usage And Synthesis
SynthesisMethyl /rara-3-amino-cyclobutanecarboxylate hydrochloride (39.94 g, 241 mmol) was suspended in dichloromethane (400 ml). The solution was cooled to 0°C before Et3N (4 equiv., 134 ml, 965 mmol) and Boc anhydride (1.2 equiv., 63.2 g, 289 mmol) were added. The cooling bath was removed and the mixture was stirred while slowly allowing to warm up to room temperature. After 20 hours of stirring, the salts were filtered off and the filtrate was rinsed three times with water. The organic layer was dried over sodium sulfate, filtered and concentrated in vacuo. The residue was triturated in heptane, the solid was filtered off and dried in air flow to give Methyl trans-3-(boc-amino)cyclobutanecarboxylate as a white solid.
Cyclobutanecarboxylic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, trans-
Methyl trans-3-(boc-amino)cyclobutanecarboxylate Preparation Products And Raw materials
Tag:Methyl trans-3-(boc-amino)cyclobutanecarboxylate(1101173-77-6) Related Product Information
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