Indanorex

Indanorex Suppliers list
Company Name: Alchem Pharmtech,Inc.
Tel: 8485655694
Email: sales@alchempharmtech.com
Products Intro: Product Name:2-(1-Aminopropyl)-2,3-dihydro-1H-inden-2-ol
CAS:16112-96-2
Purity:97+% Package:1g;10g;100g;;1kg Remarks:Z-36131
Company Name: TargetMol Chemicals Inc.
Tel: +1-781-999-5354 +1-00000000000
Email: marketing@targetmol.com
Products Intro: Product Name:Indanorex;Indanorexum;JL11698;JL 11698;JL-11698;Dietor
CAS:16112-96-2
Package:100 mg;500 mg Remarks:REAGENT;FOR LABORATORY USE ONLY
Company Name: TargetMol Chemicals Inc.
Tel: +8613564774135
Email: zijue.cai@tsbiochem.com
Products Intro: Product Name:Indanorex
CAS:16112-96-2
Package:100mg;2500USD|25mg;1520USD|50mg;1980USD
Company Name: TargetMol Chemicals Inc.  
Tel: 15002134094
Email: marketing@targetmol.cn
Products Intro: Product Name:Indanorex
CAS:16112-96-2
Package:100mg/RMB 17500;25mg/RMB 10600;50mg/RMB 13800
Company Name: Leancare Ltd.  
Tel: +33 962096793
Email: enquiry@leancare.co.uk
Products Intro:

Indanorex manufacturers

  • Indanorex
  • Indanorex pictures
  • $2500.00 / 100mg
  • 2024-10-28
  • CAS:16112-96-2
  • Min. Order:
  • Purity:
  • Supply Ability: 10g
Indanorex Basic information
Product Name:Indanorex
Synonyms:Indanorex;2-(1-Aminopropyl)indan-2-ol;Dietor;JL-11698;2-(1-Aminopropyl)-2,3-dihydro-1H-inden-2-ol;1H-Inden-2-ol, 2-(1-aminopropyl)-2,3-dihydro-;Indanorexum
CAS:16112-96-2
MF:C12H17NO
MW:191.27
EINECS:
Product Categories:
Mol File:16112-96-2.mol
Indanorex Structure
Indanorex Chemical Properties
Safety Information
MSDS Information
Indanorex Usage And Synthesis
OriginatorIndanorex,Shanghai Lansheng
Manufacturing Process125 g (1.15 mol) trimethylchlorosilane was added to 159 g (1 mol) 2-cyano- 2-hydroxyindane in 600 ml pyridine by stirring for 2 hours, whereupon the mixture was heated at 1 hour at 40°C for 1 hour. TA light precipitate was filtered off and washed with 1 liter of benzene. The filtrate was washed with water, dried over magnesium sulfate and concentrated in vacuum. The residue was dissolved in benzene 2 times and 2 times the solvent was removed in vacuum in order to any pyridine and water was present. Yield of silano_x0002_organic compound as a clear brown liquid was 230 g (100%); BP: 95°C/15 mm Hg.
10.5 g magnesium in 30 ml of dry ether was mixed with 55.5 g of ethyl bromide in 62 ml ether during about 1 hour at the temperature of boiling ether. After that the mixture was heated to 45°C in order to finish the synthesis of ethyl magnesium bromide. On cooling to 0°C it was stood for 2 hours and 50 g the above prepared silano-organic compound in 620 ml ether was added at the temperature about 5°C, whereupon in was stirred else 30 minutes at the ambient temperature and then was placed into ice bath. 82 ml of methanol was added to the prepared mixture during 1 hour. The temperature was kept about 18°C. On 30 minutes stirring the mixture was evaporated to 1/3 volume in vacuum at the temperature about 20°C. The residue was with ethanol diluted, the ethanol was evaporated, whereupon 100 ml methanol was added. 16.4 g sodium borohydride was added to the methanol solution for 1 hour at ice cooling, and stirred 2 hours at 3°C. It stood at ambient temperature overnight. Then the mixture was cooled to 10°C. 250 ml of hydrochloric acid (conc.) was added. After that it was heated at 45°C for 1 hour. The solvent was removed to dryness in vacuum. The pasty residue was in 250 ml of water dissolved and with chloroform washed. The 2- (1-aminopropyl)-2-indanol was precipitated by adding of 750 ml 10% sodium carbonate to pH 10. It was extracted with chloroform and dried over magnesium sulfate.
Chloroform was evaporated to give 13 g desired 2-(1-aminopropyl)-2-indanol. MP: 92°C. Yield 33%. IR spectrum and thin layer chromatography confirmed the structure of prepared compound.
Therapeutic FunctionAnorexic
Indanorex Preparation Products And Raw materials
Raw materialsMagnesium-->Pyridine-->Bromoethane-->Sodium borohydride-->Chlorotrimethylsilane
Tag:Indanorex(16112-96-2) Related Product Information
INDAN-2-YL-METHYLAMINE HYDROCHLORIDE Indanorex 2-Indanol