2-Allyloxy-1,3,5-tribromobenzene manufacturers
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| 2-Allyloxy-1,3,5-tribromobenzene Basic information |
Product Name: | 2-Allyloxy-1,3,5-tribromobenzene | Synonyms: | 1,3,5-tribromo-2-(2-propenyloxy)-benzen;ALLYL 2,4,6-TRIBROMOPHENYL ETHER;ALLYL TRIBROMOPHENYL ETHER;Benzene,1,3,5-tribromo-2-(2-propenyloxy);TRIBROMOPHENYL ALLYL ETHER;2-allyloxy-1,3,5-tribromobenzene;1,3,5-TribroMo-2-(2-propen-1-yloxy)-benzene;Allyl 2,4,6-tribromophenyl ether 98% | CAS: | 3278-89-5 | MF: | C9H7Br3O | MW: | 370.86 | EINECS: | 221-913-2 | Product Categories: | Allyl Monomers;Monomers;Polymer Science | Mol File: | 3278-89-5.mol | ![2-Allyloxy-1,3,5-tribromobenzene Structure](CAS/GIF/3278-89-5.gif) |
| 2-Allyloxy-1,3,5-tribromobenzene Chemical Properties |
Melting point | 74-76 °C (lit.) | Boiling point | 339.5±37.0 °C(Predicted) | density | 1.950±0.06 g/cm3(Predicted) | solubility | Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly) | form | Solid | color | Off-White to Beige | EPA Substance Registry System | Allyl 2,4,6-tribromophenyl ether (3278-89-5) |
| 2-Allyloxy-1,3,5-tribromobenzene Usage And Synthesis |
Application | 1,3,5-Tribromo-2-(2-propen-1-yloxy)-benzene is used as a brominated flame retardant. Not a dangerous good if item is equal to or less than 1g/ml and there is less than 100g/ml in the package. | Synthesis | ![Synthesis_3278-89-5](/NewsImg/2022-03-02/6378183256692037289619676.jpg) To the ethanol solution of the sodium tribromophenolate salt prepared in the step 1), the dispersing agent sodium stearate 2.5 g is added.And catalyst II phenyl triethyl ammonium chloride 5.6g,The temperature is raised to 75 ?? C to reflux the reaction.Further, 1000 ml of an ethanol solution of chloropropene having a volume ratio of chloropropene to ethanol of 1:5 was slowly added thereto, and then the reaction was kept at 75 ?? C for 6.5 h until the end.Then, the temperature is lowered to 7 ?? C in sequence, and then suction filtration is performed to recover the ethanol solution.After washing the filter cake with water, the filter cake was dried at 60 ?? C.2,4,6-Tribromophenyl allyl ether was obtained as a white powdery solid in a yield of 96.2%. |
| 2-Allyloxy-1,3,5-tribromobenzene Preparation Products And Raw materials |
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