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2-Iodo-4-methoxy-1-nitrobenzene

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CAS:214279-40-0
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CAS:214279-40-0
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CAS:214279-40-0
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CAS:214279-40-0
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Products Intro: Product Name:2-iodo-4-methoxy-1-nitrobenzene
CAS:214279-40-0
Purity:98% Package:1kg,5kg,10kg
2-Iodo-4-methoxy-1-nitrobenzene Basic information
Product Name:2-Iodo-4-methoxy-1-nitrobenzene
Synonyms:3-IODO-4-NITROANISOLE;4-NITRO-3-IODOANISOLE;3-Iodo-4-nitroanisole,97%;2-Iodo-4-Methoxy-1-nitrobenzene;3-Iodo-4-nitroanisole, 97% 5GR;2-Iodo-4-methoxy-1-nitrobenzene, 3-Iodo-4-nitrophenyl methyl ether;3-Iodo-4-nitroanisol;Benzene, 2-iodo-4-methoxy-1-nitro-
CAS:214279-40-0
MF:C7H6INO3
MW:279.03
EINECS:
Product Categories:Aromatic Ethers
Mol File:214279-40-0.mol
2-Iodo-4-methoxy-1-nitrobenzene Structure
2-Iodo-4-methoxy-1-nitrobenzene Chemical Properties
Melting point 68-73 °C
Boiling point 352.1±27.0 °C(Predicted)
density 1.9259 (estimate)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
form Crystals or Crystalline Powder
color Yellow to orange-brown
InChIInChI=1S/C7H6INO3/c1-12-5-2-3-7(9(10)11)6(8)4-5/h2-4H,1H3
InChIKeyNLTAHTYBZZSCIT-UHFFFAOYSA-N
SMILESC1([N+]([O-])=O)=CC=C(OC)C=C1I
Safety Information
Hazard Codes Xn
Risk Statements 36-33-20/21/22
Safety Statements 36/37-22
HS Code 29093090
MSDS Information
ProviderLanguage
ACROS English
2-Iodo-4-methoxy-1-nitrobenzene Usage And Synthesis
Chemical Propertiesyellow to orange-brown crystals or
SynthesisSilak reaction tube equipped with a magnetic stirrer was charged with 6.2 mg of silver sulfate,21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline,39.4 mg of 2-nitro-5-methoxybenzoic acid and 45 mg of sodium iodide4 mL of dimethyl sulfoxide. The reaction was heated at 160 ° C for 24 hours with oxygen. After the reaction, distilled water was added to quench the reaction. Extraction with ethyl acetate 3 times, each time 10mL. The combined organic phases are concentrated; 35.2 mg of 2-Iodo-4-methoxy-1-nitrobenzene was obtained in a yield of 63 percent.
2-Iodo-4-methoxy-1-nitrobenzene Preparation Products And Raw materials
Raw materials5-Methoxy-2-nitrobenzoic acid-->5-METHOXY-2-NITROANILINE
Tag:2-Iodo-4-methoxy-1-nitrobenzene(214279-40-0) Related Product Information
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