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| 2-Iodo-4-methoxy-1-nitrobenzene Basic information |
Product Name: | 2-Iodo-4-methoxy-1-nitrobenzene | Synonyms: | 3-IODO-4-NITROANISOLE;4-NITRO-3-IODOANISOLE;3-Iodo-4-nitroanisole,97%;2-Iodo-4-Methoxy-1-nitrobenzene;3-Iodo-4-nitroanisole, 97% 5GR;2-Iodo-4-methoxy-1-nitrobenzene, 3-Iodo-4-nitrophenyl methyl ether;3-Iodo-4-nitroanisol;Benzene, 2-iodo-4-methoxy-1-nitro- | CAS: | 214279-40-0 | MF: | C7H6INO3 | MW: | 279.03 | EINECS: | | Product Categories: | Aromatic Ethers | Mol File: | 214279-40-0.mol | ![2-Iodo-4-methoxy-1-nitrobenzene Structure](CAS/GIF/214279-40-0.gif) |
| 2-Iodo-4-methoxy-1-nitrobenzene Chemical Properties |
Melting point | 68-73 °C | Boiling point | 352.1±27.0 °C(Predicted) | density | 1.9259 (estimate) | storage temp. | Keep in dark place,Sealed in dry,Room Temperature | form | Crystals or Crystalline Powder | color | Yellow to orange-brown | InChI | InChI=1S/C7H6INO3/c1-12-5-2-3-7(9(10)11)6(8)4-5/h2-4H,1H3 | InChIKey | NLTAHTYBZZSCIT-UHFFFAOYSA-N | SMILES | C1([N+]([O-])=O)=CC=C(OC)C=C1I |
Provider | Language |
ACROS
| English |
| 2-Iodo-4-methoxy-1-nitrobenzene Usage And Synthesis |
Chemical Properties | yellow to orange-brown crystals or | Synthesis | Silak reaction tube equipped with a magnetic stirrer was charged with 6.2 mg of silver sulfate,21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline,39.4 mg of 2-nitro-5-methoxybenzoic acid and 45 mg of sodium iodide4 mL of dimethyl sulfoxide. The reaction was heated at 160 ° C for 24 hours with oxygen. After the reaction, distilled water was added to quench the reaction. Extraction with ethyl acetate 3 times, each time 10mL. The combined organic phases are concentrated; 35.2 mg of 2-Iodo-4-methoxy-1-nitrobenzene was obtained in a yield of 63 percent. |
| 2-Iodo-4-methoxy-1-nitrobenzene Preparation Products And Raw materials |
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