| Company Name: |
Capot Chemical Co.,Ltd. |
| Tel: |
571-85586718 +8613336195806 |
| Email: |
sales@capotchem.com |
| Products Intro: |
Product Name:4-Methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile
CAS:863868-22-8
Purity:98%(Min,HPLC) Package:100g;1kg;5kg,10kg,25kg,50kg
|
|
|
|
|
| Company Name: |
ShangHai AmK Pharmaceutical Technology Co., Ltd.
|
| Tel: |
18019252918 |
| Email: |
sale@amkchem.com |
| Products Intro: |
Product Name:4-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile
CAS:863868-22-8
Purity:0.97 Package:1g,10g,100g
|
|
| | 4-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile Basic information |
| Product Name: | 4-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile | | Synonyms: | 4-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile;Benzonitrile, 4-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)- | | CAS: | 863868-22-8 | | MF: | C14H18BNO2 | | MW: | 243.11 | | EINECS: | | | Product Categories: | | | Mol File: | 863868-22-8.mol |  |
| | 4-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile Chemical Properties |
| | 4-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile Usage And Synthesis |
| Chemical Properties | White-Yellow Crystalline Powder | | Preparation | In a glove box, a 100 mL schlenk flask, equipped with a magnetic stirring bar, was charged with Pd2(dba)3 (13.8 mg, 0.015 mmol, 3 mol % Pd) and tricyclohexylphosphine (PCy3, 20.2 mg, 0.072 mmol, 7.2 mol %). Dioxane (6 mL) was added and the resulting mixture was stirred for 30 minutes at room temperature. B2Pin2 (280 mg, 1.1 mmol), KOAc (147 mg, 1.5 mmol), and 2-bromo-4-methylbenzonitrile (196 mg, 1 mmol) were added successively. The schlenk flask was brought to a schlenk line. A condenser was attached, and the flask was flushed with nitrogen. The reaction mixture was stirred at 80° C for 12 h to obtain crude product 4-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile.
 |
| | 4-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-benzonitrile Preparation Products And Raw materials |
|