3-anilino-2-chloro-1,4-naphthoquinone(1090-16-0) ¹³C NMR

Mass

MS-NW-7737          
2-anilino-3-chloro-1,4-naphthoquinone
C16H10ClNO2         (Mass of molecular ion:    283)

   Source Temperature: 170 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      27.0       1.4
      38.0       1.5
      39.0       5.7
      50.0       9.2
      51.0      19.1
      52.0       2.4
      62.0       2.7
      63.0       4.3
      64.0       1.5
      65.0       2.3
      66.0       1.5
      73.0       1.0
      74.0       4.1
      75.0       6.0
      76.0      17.8
      77.0      39.7
      78.0       5.5
      82.5       1.3
      87.0       2.4
      88.0       4.8
      89.0       7.7
      90.0       1.1
      95.5       2.9
      96.0       1.0
      99.0       4.0
     100.0       1.3
     101.0       1.9
     104.0       8.4
     105.0      18.3
     106.0       1.3
     111.0       1.0
     114.0       4.3
     115.0       2.8
     116.0       1.5
     123.0       4.0
     124.0       1.0
     125.0       1.4
     126.0       1.5
     135.0       3.1
     137.0       1.1
     139.0       1.0
     141.5       1.1
     144.0       3.3
     150.0       1.1
     151.0       1.6
     152.0       1.7
     153.0       1.2
     154.0       1.4
     163.0       3.0
     164.0       3.6
     165.0      15.3
     166.0       2.6
     170.0       2.0
     180.0       2.7
     190.0       6.6
     191.0       5.8
     192.0       2.3
     193.0       2.1
     203.0       1.2
     219.0       5.1
     220.0       5.0
     221.0       1.8
     247.0       4.7
     248.0     100.0
     249.0      19.1
     250.0       2.1
     282.0       2.2
     283.0      71.3
     284.0      14.1
     285.0      24.3
     286.0       4.8

Assign. Shift(ppm) A 9.32 B 8.04 C *1 7.871 D *1 7.814 E 7.321 F 7.14 G 7.13

     Hz     ppm     Int.

   3731.45   9.337     32
   3730.71   9.335     40
   3725.83   9.323    510
   3720.21   9.309     41
   3219.12   8.055    404
   3218.14   8.053    443
   3217.53   8.051    534
   3215.82   8.047    387
   3215.45   8.046    388
   3211.55   8.036    478
   3210.08   8.033    621
   3209.72   8.032    619
   3209.11   8.030    556
   3208.25   8.028    497
   3204.71   8.019     34
   3154.54   7.894    191
   3153.20   7.890    210
   3151.49   7.886     32
   3150.15   7.883     32
   3149.78   7.882     34
   3147.09   7.875    464
   3145.75   7.872    395
   3143.31   7.866     50
   3142.82   7.864     44
   3141.97   7.862     46
   3141.48   7.861     45
   3139.53   7.856    308
   3138.06   7.853    276
   3129.76   7.832    334
   3128.30   7.828    337
   3125.98   7.822     48
   3125.49   7.821     41
   3125.12   7.820     44
   3124.51   7.819     50
   3122.19   7.813    417
   3120.85   7.809    428
   3114.75   7.794    172
   3113.28   7.791    160
   2936.28   7.348     55
   2933.96   7.342    389
   2931.27   7.335    109
   2926.27   7.323    684
   2921.39   7.310    135
   2920.78   7.309    113
   2918.21   7.302    598
   2916.14   7.297    100
   2914.18   7.292     31
   2863.40   7.165     37
   2863.04   7.164     39
   2858.64   7.153   1000
   2851.81   7.136    794
   2850.59   7.133    661
   2850.10   7.132    671
   2845.58   7.121    178
   2844.85   7.119    189
   2844.48   7.118    183