1530-12-7

9,9'-BIFLUORENE(1530-12-7) ¹H NMR

Product Name9,9'-BIFLUORENE

CAS 1530-12-7

Molecular FormulaC26H18

Molecular Weight330.42

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9,9'-BIFLUORENE(1530-12-7) <sup>1</sup>H NMR
Mass

MS-IW-0038          
9,9'-bifluorene
C26H18              (Mass of molecular ion:    330)

   Source Temperature: 210 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

     115.0       1.0
     139.0       1.4
     163.0       3.2
     164.0       3.7
     165.0     100.0
     166.0      15.6
     167.0       1.1
     330.0      15.7
     331.0       4.5

400 MHz at 65C

9,9'-BIFLUORENE(1530-12-7) <sup>1</sup>H NMR

¹H NMR	399.65 MHz
C₂₆ H₁₈	0.031 g : 0.5 ml CDCl₃ at 60 C
9,9'-bifluorene

    Assign.     Shift(ppm)

      A             7.640
      B     *1      7.229
      C     *1      7.046
      D             6.930
      E             4.798

     Hz     ppm     Int.

   3043.82   7.617    599
   3042.97   7.615    891
   3042.11   7.612    664
   3039.67   7.606     52
   3036.25   7.598    688
   3035.40   7.596   1000
   3034.55   7.594    740
   2897.34   7.250    409
   2896.36   7.248    432
   2892.33   7.238     58
   2889.89   7.232    832
   2888.92   7.229    885
   2885.38   7.220     54
   2882.32   7.213    465
   2881.35   7.210    488
   2878.66   7.203     49
   2824.58   7.068    476
   2823.49   7.065    494
   2820.68   7.058     46
   2817.02   7.049    942
   2815.92   7.046    983
   2812.99   7.039     64
   2812.26   7.037     66
   2809.57   7.031    557
   2808.47   7.028    565
   2804.81   7.019     33
   2772.95   6.939    701
   2765.26   6.920    530
   2758.79   6.904     31
   1917.60   4.799    927

(at 50.C)