2,4,6-Trimethylbenzenesulfonyl hydrazide (16182-15-3) MS
Product Name2,4,6-Trimethylbenzenesulfonyl hydrazide
CAS16182-15-3
Molecular FormulaC9H14N2O2S
Molecular Weight214.28
InChIInChI=1S/C9H14N2O2S/c1-6-4-7(2)9(8(3)5-6)14(12,13)11-10/h4-5,11H,10H2,1-3H3
InChIKey JQUBKTQDNVZHIY-UHFFFAOYSA-N
SmilesC1(S(NN)(=O)=O)=C(C)C=C(C)C=C1C
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MassMS-IW-8196 2,4,6-trimethylbenzenesulfonohydrazide C9H14N2O2S (Mass of molecular ion: 214)
Source Temperature: 150 °C Sample Temperature: 130 °C Direct, 75 eV
17.0 2.5 18.0 11.0 27.0 3.3 28.0 9.1 29.0 9.7 30.0 10.4 31.0 5.2 39.0 6.7 41.0 8.9 45.0 3.2 48.0 5.7 50.0 2.1 51.0 5.9 52.0 2.2 53.0 3.6 57.5 1.7 58.0 2.5 59.0 3.3 62.0 1.1 63.0 3.5 64.0 20.0 65.0 6.3 66.0 1.1 74.0 1.2 75.0 1.5 76.0 1.3 77.0 15.9 78.0 5.4 79.0 11.3 80.0 1.0 89.0 1.5 91.0 29.5 92.0 3.4 93.0 3.8 102.0 1.9 103.0 10.7 104.0 6.3 105.0 100.0 106.0 11.9 107.0 3.7 115.0 7.9 116.0 2.0 117.0 10.6 118.0 3.1 119.0 78.5 120.0 84.4 121.0 11.8 134.0 2.5 135.0 10.0 136.0 4.6 137.0 2.2 139.0 4.0 149.0 2.1 150.0 1.8 151.0 5.6 152.0 14.8 153.0 2.0 165.0 2.6 166.0 4.5 167.0 4.3 168.0 4.3 183.0 1.2 184.0 24.8 185.0 23.2 186.0 3.8 187.0 1.3 214.0 9.8 215.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H14 N2 O2 S 0.037 g : 0.5 ml CDCl3 2,4,6-trimethylbenzenesulfonohydrazide 
Assign. Shift(ppm)
A 6.983 B 5.85 C 3.47 D 2.645 E 2.311
Hz ppm Int.2791.02 6.984 249 2790.65 6.983 249 1388.31 3.474 24 1057.25 2.646 1000 923.58 2.311 501
in CDCl3
KBr disc
nujol mull
