9-ACETYLPHENANTHRENE(2039-77-2) IR1
Product Name9-ACETYLPHENANTHRENE
CAS2039-77-2
Molecular FormulaC16H12O
Molecular Weight220.27
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MassMS-NW-7969 9-acetylphenanthrene C16H12O (Mass of molecular ion: 220)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 2.9 43.0 5.5 51.0 1.4 62.0 1.2 63.0 1.8 74.0 2.1 75.0 4.9 76.0 1.3 81.5 1.1 82.5 1.7 87.0 2.9 87.5 1.2 88.0 16.9 88.5 7.9 89.0 1.6 94.0 1.1 94.5 2.5 95.0 1.1 98.0 1.2 99.0 1.1 100.0 1.1 101.0 1.6 102.5 4.6 109.0 1.2 110.0 6.7 110.5 1.1 126.0 1.3 149.0 1.2 150.0 5.9 151.0 10.1 152.0 2.0 165.0 1.2 174.0 3.0 175.0 4.1 176.0 29.8 177.0 61.1 178.0 10.4 179.0 1.4 189.0 2.9 190.0 1.1 191.0 1.9 205.0 100.0 206.0 16.8 207.0 1.6 219.0 1.6 220.0 62.0 221.0 11.1 222.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H12 O 0.044 g : 0.5 ml CDCl3 9-acetylphenanthrene 
Assign. Shift(ppm)
A *1 8.709 B *1 8.646 C 8.599 D 8.127 E 7.877 F 7.689 G *2 7.648 J *2 7.630 K 7.588 L 2.772
Hz ppm Int.3486.33 8.724 60 3484.50 8.719 41 3481.20 8.711 60 3479.37 8.707 42 3476.81 8.700 62 3476.56 8.700 62 3460.57 8.660 58 3458.13 8.653 33 3457.76 8.652 33 3456.05 8.648 52 3452.64 8.640 36 3450.93 8.635 63 3440.67 8.610 71 3432.74 8.590 72 3432.37 8.589 72 3247.92 8.127 189 3153.69 7.892 61 3152.95 7.890 59 3152.34 7.888 63 3145.87 7.872 72 3145.02 7.870 68 3144.53 7.869 73 3082.03 7.712 42 3080.69 7.709 43 3075.07 7.695 63 3073.61 7.691 90 3072.27 7.688 46 3066.65 7.674 61 3065.31 7.670 61 3058.47 7.653 95 3057.37 7.651 103 3056.15 7.648 81 3053.34 7.641 115 3052.86 7.639 108 3049.93 7.632 86 3048.71 7.629 96 3047.61 7.626 96 3042.97 7.615 30 3039.67 7.606 65 3038.57 7.604 65 3032.59 7.589 56 3031.74 7.586 87 3030.64 7.584 63 3024.78 7.569 42 3023.68 7.566 40 1107.79 2.772 1000
in CDCl3
KBr disc
nujol mull
