2170-09-4

N-METHYL-O-TOLUAMIDE(2170-09-4) IR2

Product NameN-METHYL-O-TOLUAMIDE

CAS 2170-09-4

Molecular FormulaC9H11NO

Molecular Weight149.19

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N-METHYL-O-TOLUAMIDE(2170-09-4) IR2
Mass

MS-IW-0862          
N-methyl-o-toluamide
C9H11NO             (Mass of molecular ion:    149)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      39.0       3.0
      41.0       1.0
      51.0       1.5
      58.0       1.6
      63.0       2.4
      65.0      12.1
      73.5       1.0
      77.0       1.1
      89.0       3.5
      90.0       4.6
      91.0      64.9
      92.0       5.2
     118.0      15.3
     119.0     100.0
     120.0       9.0
     134.0       5.1
     148.0      18.7
     149.0      68.2
     150.0       7.4

400 MHz in CDCl3

N-METHYL-O-TOLUAMIDE(2170-09-4) IR2

¹H NMR	399.65 MHz
C₉ H₁₁ N O	0.039 g : 0.5 ml CDCl₃
N-methyl-o-toluamide

    Assign.     Shift(ppm)

      A             7.26
      B             7.17
      C             7.14
      D             6.2
      E             2.897
      F             2.377
     
     J(D,E)=4.9HZ
     CONFIRMED BY LAOCN PROGRAM

     Hz     ppm     Int.

   2912.84   7.289     56
   2911.38   7.285     91
   2909.67   7.281    231
   2907.96   7.277    131
   2904.30   7.268    158
   2901.86   7.262    168
   2900.39   7.258    175
   2897.71   7.251    147
   2896.24   7.247     68
   2869.38   7.180    167
   2864.87   7.169     40
   2861.08   7.159    117
   2860.35   7.158    144
   2852.54   7.138    119
   2851.68   7.136    123
   2844.85   7.119     53
   2844.24   7.117     51
   2469.85   6.181     30
   1160.28   2.904    965
   1155.40   2.892    941
    950.20   2.378   1000

in CDCl3

KBr disc

nujol mull

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