26690-80-2

TERT-BUTYL N-(2-HYDROXYETHYL)CARBAMATE(26690-80-2) MS

Product NameTERT-BUTYL N-(2-HYDROXYETHYL)CARBAMATE

CAS 26690-80-2

Molecular FormulaC7H15NO3

Molecular Weight161.2

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TERT-BUTYL N-(2-HYDROXYETHYL)CARBAMATE(26690-80-2) MS
Mass

MS-IW-9208          
tert-butyl (2-hydroxyethyl)carbamate
C7H15NO3            (Mass of molecular ion:    161)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.6
      17.0       3.2
      18.0      16.0
      26.0       1.1
      27.0       7.3
      28.0      12.1
      29.0      19.7
      30.0      65.6
      31.0      10.3
      38.0       1.3
      39.0      12.2
      40.0       3.0
      41.0      53.0
      42.0       6.4
      43.0       6.8
      44.0      20.3
      45.0       3.5
      50.0       1.2
      51.0       1.1
      53.0       1.7
      55.0       6.9
      56.0      16.7
      57.0     100.0
      58.0       5.0
      59.0      47.9
      60.0       3.0
      61.0       2.3
      62.0       5.2
      70.0       3.3
      74.0       1.6
      75.0       3.4
      76.0       8.8
      87.0       1.5
      88.0       9.2
     105.0       4.4
     106.0       3.2
     130.0       5.0
     131.0       4.1

400 MHz in CDCl3

TERT-BUTYL N-(2-HYDROXYETHYL)CARBAMATE(26690-80-2) MS

¹H NMR	399.65 MHz
C₇ H₁₅ N O₃	0.05 ml : 0.5 ml CDCl₃
tert-butyl (2-hydroxyethyl)carbamate

    Assign.     Shift(ppm)

      A             5.45
      B             3.94
      C             3.659
      D             3.256
      E             1.442

     Hz     ppm     Int.

   2178.83   5.452     39
   1467.65   3.673    108
   1462.52   3.660    171
   1457.28   3.647    112
   1304.69   3.265     94
   1299.68   3.253     92
    576.54   1.443   1000

in CDCl3