2767-90-0

1-Pyridin-4-ylpiperidine(2767-90-0) MS

Product Name1-Pyridin-4-ylpiperidine

CAS 2767-90-0

Molecular FormulaC10H14N2

Molecular Weight162.23

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1-Pyridin-4-ylpiperidine(2767-90-0) MS
Mass

MS-NW-9941          
4-piperidinopyridine
C10H14N2            (Mass of molecular ion:    162)

   Source Temperature: 130 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      27.0       1.7
      28.0       1.8
      29.0       1.3
      39.0       2.7
      41.0       2.8
      42.0       1.6
      50.0       1.1
      51.0       7.5
      52.0       2.2
      53.0       1.2
      55.0       3.0
      65.0       1.2
      66.0       1.2
      67.0       1.1
      78.0      11.3
      79.0       2.8
      80.0       1.0
      84.0       1.3
      92.0       1.8
      93.0       1.2
     105.0      11.6
     106.0      22.2
     107.0       7.0
     119.0       2.8
     120.0       1.2
     121.0      15.6
     122.0       1.3
     131.0       1.5
     132.0       1.7
     133.0       8.5
     134.0       1.3
     145.0       1.0
     147.0       3.2
     159.0       1.6
     160.0       1.6
     161.0     100.0
     162.0      79.4
     163.0      11.5

400 MHz in CDCl3

1-Pyridin-4-ylpiperidine(2767-90-0) MS

¹H NMR	399.65 MHz
C₁₀ H₁₄ N₂	0.035 g : 0.5 ml CDCl₃
4-piperidinopyridine

    Assign.     Shift(ppm)

      A             8.225
      B             6.633
      C             3.32
      D          1.65 to 1.62

     Hz     ppm     Int.

   3290.53   8.234    263
   3284.06   8.218    265
   2654.30   6.642    415
   2652.71   6.638    292
   2649.17   6.629    301
   2647.58   6.625    399
   1331.18   3.331    321
   1326.05   3.319    519
    667.60   1.671     30
    655.52   1.641   1000
    649.17   1.625    198

in CDCl3