Fmoc-Gly-OH(29022-11-5) MS
Product NameFmoc-Gly-OH
CAS29022-11-5
Molecular FormulaC17H15NO4
Molecular Weight297.31
InChIInChI=1S/C17H15NO4/c19-16(20)9-18-17(21)22-10-15-13-7-3-1-5-11(13)12-6-2-4-8-14(12)15/h1-8,15H,9-10H2,(H,18,21)(H,19,20)
InChIKey NDKDFTQNXLHCGO-UHFFFAOYSA-N
SmilesC(O)(=O)CNC(OCC1C2=C(C=CC=C2)C2=C1C=CC=C2)=O
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MassMS-IW-2646 N-((9-fluorenyl)methoxycarbonyl)glycine C17H15NO4 (Mass of molecular ion: 297)
Source Temperature: 180 °C Sample Temperature: 150 °C Direct, 75 eV
28.0 4.4 29.0 6.2 30.0 1.5 44.0 1.8 56.0 2.1 57.0 3.1 63.0 2.5 69.5 1.3 74.0 1.8 75.0 1.6 76.0 2.4 81.5 1.2 82.0 1.1 82.5 1.9 87.0 1.5 88.0 2.3 89.0 3.3 101.0 3.9 115.0 3.1 126.0 1.2 139.0 5.0 150.0 1.1 151.0 1.9 152.0 2.8 162.0 1.3 163.0 11.0 164.0 10.0 165.0 100.0 166.0 74.9 167.0 10.4 176.0 4.3 177.0 3.4 178.0 55.4 179.0 10.4 180.0 1.0 196.0 30.8 197.0 4.8 297.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C17 H15 N O4 0.050 g : 0.5 ml DMSO-d6 N-((9-fluorenyl)methoxycarbonyl)glycine 
Assign. Shift(ppm)
A 7.900 B 7.734 C 7.67 D 7.429 E 7.348 F 4.325 G 4.252 J 3.704 J(C,J)=6.2HZ
Hz ppm Int.3161.13 7.910 914 3153.69 7.892 1000 3145.51 7.871 31 3145.26 7.871 31 3094.73 7.744 727 3087.40 7.726 816 3079.35 7.706 40 3078.61 7.704 39 3077.76 7.702 41 3077.27 7.700 42 3077.03 7.700 42 3076.78 7.699 42 3076.05 7.697 40 3075.44 7.696 37 3074.83 7.694 38 3073.85 7.692 40 3073.36 7.691 42 3069.09 7.680 190 3062.99 7.665 422 3056.88 7.649 225 2977.05 7.450 426 2969.73 7.431 963 2962.16 7.412 606 2955.44 7.396 41 2954.59 7.393 37 2952.88 7.389 31 2951.42 7.386 34 2950.56 7.383 34 2950.20 7.382 33 2947.39 7.375 108 2943.36 7.365 586 2939.94 7.357 239 2938.72 7.354 272 2935.91 7.347 875 2929.32 7.330 355 2928.47 7.328 373 1744.51 4.366 32 1744.14 4.365 32 1743.53 4.363 33 1742.68 4.361 31 1742.31 4.360 32 1741.70 4.359 32 1740.97 4.357 35 1732.67 4.336 561 1725.83 4.319 958 1718.38 4.300 72 1717.04 4.297 67 1715.70 4.294 59 1714.97 4.292 58 1714.60 4.291 56 1713.99 4.289 54 1713.26 4.287 53 1712.65 4.286 52 1711.67 4.283 51 1711.18 4.282 52 1705.32 4.268 301 1698.73 4.251 382 1698.36 4.250 383 1692.02 4.234 193 1685.67 4.218 48 1684.20 4.215 40 1683.47 4.213 38 1682.98 4.212 36 1682.37 4.210 34 1682.01 4.209 34 1681.27 4.207 32 1680.54 4.206 31 1680.05 4.204 30 1503.17 3.762 31 1502.20 3.759 32 1501.59 3.758 33 1500.24 3.754 36 1499.63 3.753 38 1499.02 3.751 39 1497.44 3.747 44 1497.07 3.746 45 1496.46 3.745 47 1495.61 3.743 50 1495.24 3.742 51 1494.75 3.741 53 1494.02 3.739 56 1493.29 3.737 60 1492.68 3.735 62 1492.31 3.735 64 1491.58 3.733 67 1490.60 3.730 71 1483.64 3.713 815 1477.42 3.697 822 1469.48 3.677 55 1468.14 3.674 49 1466.80 3.671 42 1466.19 3.669 40 1465.70 3.668 38 1465.09 3.666 35 1464.48 3.665 34 1462.77 3.661 30
in DMSO-d6
KBr disc
nujol mull
