3A,4,5,6-TETRAHYDROSUCCINIMIDO(3,4-B)-ACENAPHTHEN-10-ONE, 99(4756-92-7) 1H NMR
Molecular FormulaC14H11NO3
Molecular Weight241.24
-
MassMS-NW-8039 2-oxo-7,8-dihydro-1,8a(6H)-acenaphthenedicarboximide C14H11NO3 (Mass of molecular ion: 241)
Source Temperature: 200 °C Sample Temperature: 160 °C Direct, 75 eV
18.0 2.7 27.0 1.0 28.0 4.6 39.0 2.7 50.0 1.5 51.0 2.6 52.0 1.2 57.0 1.3 57.5 3.6 58.0 1.2 62.0 1.8 63.0 5.0 63.5 1.2 64.0 1.5 65.0 1.2 69.0 1.8 69.5 2.8 70.0 6.0 70.5 2.8 71.0 4.1 74.0 1.6 75.0 1.8 76.0 1.2 77.0 1.8 84.0 3.7 87.0 1.5 88.0 1.7 89.0 2.2 99.0 1.6 102.0 1.3 113.0 2.0 114.0 3.8 115.0 12.3 116.0 1.6 127.0 2.8 128.0 5.3 129.0 1.6 139.0 5.5 140.0 2.6 141.0 26.8 142.0 21.0 143.0 2.5 155.0 2.6 156.0 1.2 169.0 7.6 170.0 100.0 171.0 13.1 172.0 1.1 198.0 1.7 199.0 1.7 241.0 30.1 242.0 4.9
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C14 H11 N O3 0.031 g : 0.5 ml DMSO-d6 2-oxo-7,8-dihydro-1,8a(6H)-acenaphthenedicarboximide 
Assign. Shift(ppm)
A 11.33 B 7.587 C 7.523 D 7.497 E 3.955 F *1 3.184 G *1 2.785 J 2.44 K 1.814
Hz ppm Int.4528.24 11.331 75 3036.53 7.598 170 3029.57 7.581 240 3011.62 7.536 123 3005.21 7.520 347 3000.63 7.509 447 2993.67 7.491 311 2985.98 7.472 118 1580.73 3.956 1000 1287.48 3.222 46 1282.17 3.209 52 1280.52 3.205 53 1280.15 3.204 53 1275.94 3.193 52 1270.26 3.179 59 1266.23 3.169 70 1263.30 3.162 62 1258.35 3.149 63 1127.02 2.821 53 1120.98 2.805 86 1120.06 2.803 86 1114.39 2.789 64 1110.17 2.778 45 1104.13 2.763 79 1097.17 2.746 58 1011.45 2.531 39 1007.97 2.523 262 1006.32 2.519 534 1002.65 2.509 556 1001.00 2.505 283 996.98 2.495 61 994.78 2.490 50 990.56 2.479 54 987.08 2.470 73 984.15 2.463 81 981.22 2.456 121 977.74 2.447 189 971.88 2.432 96 968.40 2.424 149 961.81 2.407 77 741.09 1.855 57 735.05 1.840 86 731.93 1.832 142 726.44 1.818 177 721.86 1.807 178 720.94 1.804 172 716.91 1.794 69 714.72 1.789 52 712.52 1.783 83 707.76 1.771 40
in DMSO-d6
KBr disc
nujol mull
