1,8-Dichloro-9,10-bis(phenylethynyl) anthracene(51749-83-8) IR2
Product Name1,8-Dichloro-9,10-bis(phenylethynyl) anthracene
CAS51749-83-8
Molecular FormulaC30H16Cl2
Molecular Weight447.35
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MassMS-NW-8357 1,8-dichloro-9,10-bis(phenylethynyl)anthracene C30H16Cl2 (Mass of molecular ion: 446)
Source Temperature: 220 °C Sample Temperature: 240 °C Direct, 75 eV
17.0 4.0 18.0 7.3 27.0 4.7 28.0 8.6 29.0 2.5 38.0 4.9 39.0 11.2 41.0 3.8 43.0 2.6 44.0 5.3 45.0 2.6 49.0 2.4 50.0 4.5 51.0 8.0 57.0 3.1 62.0 2.9 63.0 6.6 65.0 8.7 74.0 2.9 77.0 3.6 89.0 3.3 91.0 52.1 92.0 36.7 93.0 4.2 149.0 2.6 150.0 3.4 161.0 3.2 173.0 2.9 174.0 5.2 185.0 2.8 186.0 5.5 187.0 10.5 187.5 4.5 188.0 4.1 222.0 2.6 223.0 10.0 223.5 2.5 224.0 5.9 248.0 2.4 276.0 4.0 278.0 2.7 298.0 3.3 300.0 3.2 322.0 2.7 346.0 3.8 348.0 5.3 350.0 3.2 370.0 2.5 372.0 10.9 373.0 6.2 374.0 27.0 375.0 13.0 376.0 23.7 377.0 5.9 378.0 6.4 408.0 2.4 410.0 10.0 411.0 3.3 412.0 33.6 413.0 10.6 414.0 12.1 415.0 4.0 446.0 100.0 447.0 31.7 448.0 72.7 449.0 21.5 450.0 14.8 451.0 4.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C30 H16 Cl2 saturated in CDCl3 1,8-dichloro-9,10-bis(phenylethynyl)anthracene 
Assign. Shift(ppm)
A 8.539 B 7.67 C 7.65 D 7.41 E 7.39 F 7.35
Hz ppm Int.3417.97 8.553 337 3416.75 8.550 395 3409.30 8.531 371 3408.08 8.528 406 3075.44 7.696 222 3074.58 7.694 185 3073.24 7.690 173 3070.80 7.684 525 3069.09 7.680 439 3068.12 7.678 425 3065.80 7.672 308 3064.21 7.668 257 3062.50 7.663 468 3061.04 7.660 686 3059.94 7.657 478 3053.83 7.642 440 3052.73 7.639 473 2975.22 7.445 38 2974.37 7.443 40 2973.63 7.441 39 2969.85 7.432 462 2967.53 7.426 144 2965.70 7.421 370 2963.99 7.417 436 2962.65 7.414 530 2961.18 7.410 1000 2958.86 7.404 697 2953.98 7.392 450 2952.51 7.388 458 2950.93 7.384 213 2946.53 7.373 196 2945.07 7.370 354 2943.60 7.366 200 2941.89 7.362 279 2940.31 7.358 157 2937.87 7.352 85 2935.30 7.345 159 2934.81 7.344 161 2931.15 7.335 38 2929.08 7.330 39 2927.61 7.326 51
KBr disc
nujol mull
