5814-05-1

2-Chlorobenzhydrazide(5814-05-1) ¹³C NMR

Product Name2-Chlorobenzhydrazide

CAS 5814-05-1

Molecular FormulaC7H7ClN2O

Molecular Weight170.6

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2-Chlorobenzhydrazide(5814-05-1) <sup>13</sup>C NMR
Mass

MS-IW-6307          
o-chlorobenzohydrazide
C7H7ClN2O           (Mass of molecular ion:    170)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      31.0       1.1
      50.0       3.5
      51.0       2.4
      74.0       2.0
      75.0      11.9
      76.0       2.7
      77.0       1.2
      85.0       1.3
     111.0      34.0
     112.0       2.5
     113.0      11.1
     139.0     100.0
     140.0       7.8
     141.0      32.0
     142.0       2.5
     170.0      21.4
     171.0       2.5
     172.0       7.0

400 MHz in DMSO-d6

2-Chlorobenzhydrazide(5814-05-1) <sup>13</sup>C NMR

¹H NMR	399.65 MHz
C₇ H₇ Cl N₂ O	0.040 g : 0.5 ml DMSO-d₆
o-chlorobenzohydrazide

    Assign.     Shift(ppm)

      A             9.58
      B             7.489
      C             7.44
      D             7.39
      E             4.51

     Hz     ppm     Int.

   3829.96   9.584    209
   2999.73   7.506    176
   2998.81   7.504    300
   2997.89   7.502    212
   2991.79   7.487    417
   2991.18   7.485    530
   2990.57   7.483    487
   2989.96   7.482    432
   2986.91   7.474     44
   2982.33   7.463    240
   2978.97   7.454    305
   2976.84   7.449    292
   2973.48   7.441    405
   2971.19   7.435    139
   2968.75   7.429    185
   2965.55   7.421    258
   2960.51   7.408     59
   2957.92   7.402    138
   2957.31   7.400    165
   2953.49   7.391   1000
   2953.03   7.390    927
   2952.42   7.388    740
   2950.44   7.383    456
   2949.83   7.382    423
   2947.85   7.377    357
   2946.62   7.374    320
   2942.35   7.363     31
   2940.37   7.358     69
   2939.15   7.355     61
   1801.45   4.508    616

in CDCl3

in DMSO-d6